2-[8-(tetrahydro-2H-pyran-2-yloxy)octyloxy]-4-(3-trifluoromethyl-3H-diazirin-3-yl)benzyl methanesulfonate

Base Information

Chemical Name:2-[8-(tetrahydro-2H-pyran-2-yloxy)octyloxy]-4-(3-trifluoromethyl-3H-diazirin-3-yl)benzyl methanesulfonate
CAS No.:943601-15-8
Molecular Formula:C₂₃H₃₃F₃N₂O₆S
Molecular Weight:522.586
Hs Code.:

Synonyms:2-[8-(tetrahydro-2H-pyran-2-yloxy)octyloxy]-4-(3-trifluoromethyl-3H-diazirin-3-yl)benzyl methanesulfonate

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Chemical Property of 2-[8-(tetrahydro-2H-pyran-2-yloxy)octyloxy]-4-(3-trifluoromethyl-3H-diazirin-3-yl)benzyl methanesulfonate

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Technology Process of 2-[8-(tetrahydro-2H-pyran-2-yloxy)octyloxy]-4-(3-trifluoromethyl-3H-diazirin-3-yl)benzyl methanesulfonate

There total 4 articles about 2-[8-(tetrahydro-2H-pyran-2-yloxy)octyloxy]-4-(3-trifluoromethyl-3H-diazirin-3-yl)benzyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 943601-14-7
C₂₂H₃₁F₃N₂O₄

: 124-63-0
methanesulfonyl chloride

: 943601-15-8
2-[8-(tetrahydro-2H-pyran-2-yloxy)octyloxy]-4-(3-trifluoromethyl-3H-diazirin-3-yl)benzyl methanesulfonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.166667h;
DOI:10.1021/ol070376i

Reference yield:

: 943601-13-6
2-{[8-(tetrahydropyran-2-yloxy)-octyloxy]-4-(3-trifluoromethyl-3H-diazirin-3-yl)}-benzaldehyde

: 943601-15-8
2-[8-(tetrahydro-2H-pyran-2-yloxy)octyloxy]-4-(3-trifluoromethyl-3H-diazirin-3-yl)benzyl methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 822 mg / sodium borohydride / ethanol / 0.17 h / 0 °C

2: 93 percent / triethylamine / CH₂Cl₂ / 0.17 h / 0 °C

With sodium tetrahydroborate; triethylamine; In ethanol; dichloromethane;
DOI:10.1021/ol070376i

Reference yield:

: 50816-20-1
2-(8-bromooctyloxy)tetrahydropyran

: 943601-15-8
2-[8-(tetrahydro-2H-pyran-2-yloxy)octyloxy]-4-(3-trifluoromethyl-3H-diazirin-3-yl)benzyl methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; tetra-n-butylammonium iodide / dimethylformamide / 1 h / 60 °C

2: 822 mg / sodium borohydride / ethanol / 0.17 h / 0 °C

3: 93 percent / triethylamine / CH₂Cl₂ / 0.17 h / 0 °C

With sodium tetrahydroborate; tetra-(n-butyl)ammonium iodide; potassium carbonate; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol070376i