bis(ethoxycarbonyl)(phenyliodinio)methanide

Base Information

Chemical Name:bis(ethoxycarbonyl)(phenyliodinio)methanide
CAS No.:15277-68-6
Molecular Formula:C₁₃H₁₅IO₄
Molecular Weight:362.164
Hs Code.:

Synonyms:bis(ethoxycarbonyl)(phenyliodinio)methanide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(ethoxycarbonyl)(phenyliodinio)methanide

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Technology Process of bis(ethoxycarbonyl)(phenyliodinio)methanide

There total 2 articles about bis(ethoxycarbonyl)(phenyliodinio)methanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 3240-34-4
[bis(acetoxy)iodo]benzene

: 105-53-3
diethyl malonate

: 15277-68-6
bis(ethoxycarbonyl)(phenyliodinio)methanide

Guidance literature:: diethyl malonate; With potassium hydroxide; In dichloromethane; at 20 ℃; for 0.0833333h; Inert atmosphere;

[bis(acetoxy)iodo]benzene; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo802208q

Reference yield:

: 64-17-5
ethanol

: 3240-34-4
[bis(acetoxy)iodo]benzene

: 105-53-3
diethyl malonate

: 15277-68-6
bis(ethoxycarbonyl)(phenyliodinio)methanide

Guidance literature:: With potassium hydroxide;

Reference yield: 84.0%

: 15277-68-6
bis(ethoxycarbonyl)(phenyliodinio)methanide

: 284042-73-5
3-benzoyl-5-methyl-1-vinylpyrimidine-2,4(1H, 3H)-dione

: (R)-diethyl 2-(3-benzoyl-5-methyl-2,4-dioxo-3,4-dihydropyrimidin-1(2H)-yl)cyclopropane-1,1-dicarboxylate

Guidance literature:: With (4S,4's)-2,2'-(1,3-bis(4-(tert-butyl)phenyl)propane-2,2-diyl)bis(4-phenyl-4,5-dihydro-oxazole); copper(II) bis(trifluoromethanesulfonate); at -20 ℃; for 72h; enantioselective reaction; Inert atmosphere; Schlenk technique; Molecular sieve;
DOI:10.1039/d0cc04536e