4-methoxybenzyl 5-chloro-1-ethyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate

Base Information

Chemical Name:4-methoxybenzyl 5-chloro-1-ethyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate
CAS No.:1429439-23-5
Molecular Formula:C₃₆H₃₄ClNO₈
Molecular Weight:644.121
Hs Code.:

Synonyms:4-methoxybenzyl 5-chloro-1-ethyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate

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Chemical Property of 4-methoxybenzyl 5-chloro-1-ethyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate

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Technology Process of 4-methoxybenzyl 5-chloro-1-ethyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate

There total 4 articles about 4-methoxybenzyl 5-chloro-1-ethyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 80104-60-5
5-chloro-6,7-dihydroxy-1,4-dihydro-1-ethyl-4-oxoquinoline-3-carboxylic acid

: 824-94-2
p-methoxybenzyl chloride

: 1429439-23-5
4-methoxybenzyl 5-chloro-1-ethyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 90 ℃; for 4h; Inert atmosphere;

Reference yield:

: 14698-29-4
oxolinic Acid

: 1429439-23-5
4-methoxybenzyl 5-chloro-1-ethyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid; potassium nitrate / 1 h / 0 - 20 °C / Inert atmosphere

2: hydrogenchloride; palladium on activated charcoal; hydrogen; acetic acid / 1 h / 2585.81 Torr

3: hydrogenchloride; sodium nitrite / water / 5 h / 20 - 45 °C / Inert atmosphere

4: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 4 h / 90 °C / Inert atmosphere

With hydrogenchloride; sulfuric acid; palladium on activated charcoal; hydrogen; potassium carbonate; acetic acid; potassium nitrate; potassium iodide; sodium nitrite; In water; N,N-dimethyl-formamide;

Reference yield:

: 51624-54-5
9-amino-5-ethyl-8-oxo-5,8-dihydro-[1,3]dioxolo[4,5-g]quinolin-7-carboxylic acid

: 1429439-23-5
4-methoxybenzyl 5-chloro-1-ethyl-6,7-bis((4-methoxybenzyl)oxy)-4-oxo-1,4-dihydroquinolin-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; sodium nitrite / water / 5 h / 20 - 45 °C / Inert atmosphere

2: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 4 h / 90 °C / Inert atmosphere

With hydrogenchloride; potassium carbonate; potassium iodide; sodium nitrite; In water; N,N-dimethyl-formamide;