Mo(VI)(N-2,6-cl2C₆H₃)2(Cl₂)dimethoxyethane

Base Information

Chemical Name:Mo(VI)(N-2,6-cl2C₆H₃)2(Cl₂)dimethoxyethane
CAS No.:259267-54-4
Molecular Formula:C₁₆H₁₆Cl₆MoN₂O₂
Molecular Weight:576.973
Hs Code.:

Mo(VI)(N-2,6-cl2C<sub>6</sub>H<sub>3</sub>)2(Cl<sub>2</sub>)dimethoxyethane

Synonyms:Mo(VI)(N-2,6-cl2C₆H₃)2(Cl₂)dimethoxyethane

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Chemical Property of Mo(VI)(N-2,6-cl2C₆H₃)2(Cl₂)dimethoxyethane

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Technology Process of Mo(VI)(N-2,6-cl2C₆H₃)2(Cl₂)dimethoxyethane

There total 2 articles about Mo(VI)(N-2,6-cl2C₆H₃)2(Cl₂)dimethoxyethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: sodium molybdate

: 75-77-4
chloro-trimethyl-silane

: 110-71-4
1,2-dimethoxyethane

: 608-31-1
2,6-Dichloroaniline

: 259267-54-4
molybdenum(VI) bis(NC₆H₃Cl₂-2,6)Cl₂(1,2-dimethoxyethane)

Guidance literature:: With NEt₃; In 1,2-dimethoxyethane; (N2); addn. of DME to anhydrous sodium molybdate, to this suspn. was added NEt3, Me3SiCl and the amine, stirring (65°C, 18 h); filtration, removal of volatiles (reduced pressure), washing (light petroleum), drying (vac.), redissoln. (min. amt. Et2O), filtration, crystn. on cooling to -20°C, collection, drying;
DOI:10.1039/a907382e

Reference yield: 90.0%

: sodium molybdate

: 75-77-4
chloro-trimethyl-silane

: 608-31-1
2,6-Dichloroaniline

: 259267-54-4
Mo(VI)(N-2,6-cl2C₆H₃)2(Cl₂)dimethoxyethane

Guidance literature:: With triethylamine; In 1,2-dimethoxyethane; byproducts: [(CH3)3Si]2O, NaCl, (C2H5)3NHCl; (Ar), mixed with suspn. of Mo complex, treated with chloromethylsilane, stirred under reflux for 18 h, cooled to room temp.; filtered, washed (DME), evapd.(vac.), cooled to 0°C, elem. anal.,NMR, MAS, XRD;
DOI:10.1016/S0277-5387(00)00605-7

Reference yield: 75.0%

: 147-84-2
Diethyldithiocarbamic acid

: 259267-54-4
molybdenum(VI) bis(NC₆H₃Cl₂-2,6)Cl₂(1,2-dimethoxyethane)

: 174281-08-4
[Mo(NC₆H₃Cl₂)2(S₂CN(C₂H₅)2)2]

Guidance literature:: In diethyl ether; (N2); stirring (room temp., 16 h); filtration, washing (Et2O), concn. (reduced pressure), crystn. on cooling to -20°C, filtration, washing (light petroleum), drying (vac.);elem. anal.;
DOI:10.1039/a907382e