(S)-tert-butyl (2-((6-(4-chlorophenyl)-4-(2-(ethylamino)-2-oxoethyl)-1-methyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-8-yl)oxy)ethyl)carbamate

Base Information

Chemical Name:(S)-tert-butyl (2-((6-(4-chlorophenyl)-4-(2-(ethylamino)-2-oxoethyl)-1-methyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-8-yl)oxy)ethyl)carbamate
CAS No.:1426687-02-6
Molecular Formula:C₂₈H₃₃ClN₆O₄
Molecular Weight:553.061
Hs Code.:

Synonyms:(S)-tert-butyl (2-((6-(4-chlorophenyl)-4-(2-(ethylamino)-2-oxoethyl)-1-methyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-8-yl)oxy)ethyl)carbamate

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Chemical Property of (S)-tert-butyl (2-((6-(4-chlorophenyl)-4-(2-(ethylamino)-2-oxoethyl)-1-methyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-8-yl)oxy)ethyl)carbamate

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Technology Process of (S)-tert-butyl (2-((6-(4-chlorophenyl)-4-(2-(ethylamino)-2-oxoethyl)-1-methyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-8-yl)oxy)ethyl)carbamate

There total 12 articles about (S)-tert-butyl (2-((6-(4-chlorophenyl)-4-(2-(ethylamino)-2-oxoethyl)-1-methyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-8-yl)oxy)ethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1300746-10-4
2-((4S)-6-(4-chlorophenyl)-8-hydroxy-1-methyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-4-yl)-N-ethylacetamide

: 96628-67-0
2-(tert-butoxycarbonylamino)ethyl methanesulfonate

: 1426687-02-6
(S)-tert-butyl (2-((6-(4-chlorophenyl)-4-(2-(ethylamino)-2-oxoethyl)-1-methyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-8-yl)oxy)ethyl)carbamate

Guidance literature:: 2-((4S)-6-(4-chlorophenyl)-8-hydroxy-1-methyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-4-yl)-N-ethylacetamide; With potassium carbonate; In acetonitrile; at 81 ℃; for 0.166667h;

2-(tert-butoxycarbonylamino)ethyl methanesulfonate; In acetonitrile; at 80 ℃; for 6 - 10h;

Reference yield:

: 1260907-17-2
2-[(4S)-6-(4-chlorophenyl)-1-methyl-8-(methyloxy)-4H-[1,2,4]triazolo[4,3-a][1,4] benzodiazepin-4-yl]-N-ethylacetamide

: 1426687-02-6
(S)-tert-butyl (2-((6-(4-chlorophenyl)-4-(2-(ethylamino)-2-oxoethyl)-1-methyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-8-yl)oxy)ethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: boron tribromide / dichloromethane / 15 h / -20 - 20 °C

2: potassium carbonate / acetonitrile / 16 h / 80 °C / Inert atmosphere

With boron tribromide; potassium carbonate; In dichloromethane; acetonitrile;

Reference yield:

: 26690-80-2
2-(N-tert-butoxycarbonylamino)ethanol

: 1426687-02-6
(S)-tert-butyl (2-((6-(4-chlorophenyl)-4-(2-(ethylamino)-2-oxoethyl)-1-methyl-4H-benzo[f][1,2,4]triazolo[4,3-a][1,4]diazepin-8-yl)oxy)ethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0.17 h / 0 °C

1.2: 1 h / 20 °C

2.1: potassium carbonate / acetonitrile / 16 h / 80 °C / Inert atmosphere

With potassium carbonate; triethylamine; In dichloromethane; acetonitrile;