Methylparaben-¹³C

Base Information

Chemical Name:Methylparaben-¹³C
CAS No.:220077-36-1
Molecular Formula:C₈H₈O₃
Molecular Weight:153.139
Hs Code.:

Synonyms:Methylparaben-¹³C

Suppliers and Price of Methylparaben-¹³C

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Methylparaben-¹³C

Chemical Property:

Purity/Quality:: >98% ^*data from raw suppliers

Safty Information:

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Technology Process of Methylparaben-¹³C

There total 1 articles about Methylparaben-¹³C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 67-56-1
methanol

: 98491-29-3
1-iodo-4-(methoxymethoxy)benzene

: 1641-69-6
[13C]Carbon monoxide

: 220077-36-1
Methylparaben-¹³C

: 220077-35-0
methyl 4-(methoxymethyloxy)(carbonyl-13C)benzoate

Guidance literature:: With palladium diacetate; triethylamine; triphenylphosphine; at 120 ℃; for 24h; under 2206.5 Torr;
DOI:10.1016/S0040-4020(98)00995-8

Reference yield: 100.0%

: 107-30-2
chloromethyl methyl ether

: 220077-36-1
Methylparaben-¹³C

: 220077-35-0
methyl 4-(methoxymethyloxy)(carbonyl-13C)benzoate

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.333333h;
DOI:10.1016/S0040-4020(98)00995-8

Reference yield:

: 220077-36-1
Methylparaben-¹³C

: 129077-96-9,93627-94-2
L-[3-⁽¹³⁾C]tyrosine

Guidance literature:: Multi-step reaction with 7 steps

1: 100 percent / NaH / tetrahydrofuran / 0.33 h / 0 °C

2: 94 percent / LiAlH₄ / tetrahydrofuran / 1.5 h / 0 °C

3: 91 percent / LiBr, CH₃SO₂Cl, Et₃N / tetrahydrofuran / 1.5 h / -60 - 0 °C

4: 50 percent / sodium bis(trimethylsily)amide / tetrahydrofuran; 1,2-dimethoxy-ethane / 7 h / -78 °C

5: 100 percent / HCl / 2.5 h / Heating

6: 1.09 g / H₂ / Pd/C / ethanol / 50 h / 4413.05 Torr / Ambient temperature

7: 58 percent / aq. HCl / 4 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; hydrogen; sodium hexamethyldisilazane; sodium hydride; methanesulfonyl chloride; triethylamine; lithium bromide; palladium on activated charcoal; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol;
DOI:10.1016/S0040-4020(98)00995-8