(S,Z)-N-(1-ethoxy-1-oxo-3-phenylpropan-2-yl)-2-methylpropan-1-imine oxide

Base Information

Chemical Name:(S,Z)-N-(1-ethoxy-1-oxo-3-phenylpropan-2-yl)-2-methylpropan-1-imine oxide
CAS No.:1462968-82-6
Molecular Formula:C₁₅H₂₁NO₃
Molecular Weight:263.337
Hs Code.:

Synonyms:(S,Z)-N-(1-ethoxy-1-oxo-3-phenylpropan-2-yl)-2-methylpropan-1-imine oxide

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Chemical Property of (S,Z)-N-(1-ethoxy-1-oxo-3-phenylpropan-2-yl)-2-methylpropan-1-imine oxide

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Technology Process of (S,Z)-N-(1-ethoxy-1-oxo-3-phenylpropan-2-yl)-2-methylpropan-1-imine oxide

There total 4 articles about (S,Z)-N-(1-ethoxy-1-oxo-3-phenylpropan-2-yl)-2-methylpropan-1-imine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50547-07-4
ethyl N-hydroxy-L-phenylalaninate

: 78-84-2
isobutyraldehyde

: 1462968-82-6
(S,Z)-N-(1-ethoxy-1-oxo-3-phenylpropan-2-yl)-2-methylpropan-1-imine oxide

Guidance literature:: With magnesium sulfate; at 20 ℃; for 4h;
DOI:10.1016/j.tet.2013.08.084

Reference yield:

: 1462968-83-7
(S,Z)-N-(1-ethoxy-1-oxo-3-phenylpropan-2-yl)-1-phenylmethanimine oxide

: 1462968-82-6
(S,Z)-N-(1-ethoxy-1-oxo-3-phenylpropan-2-yl)-2-methylpropan-1-imine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; acetic acid; hydroxylamine hydrochloride / methanol / 16 h / Reflux

2: magnesium sulfate / 4 h / 20 °C

With hydroxylamine hydrochloride; magnesium sulfate; acetic acid; sodium hydroxide; In methanol;
DOI:10.1016/j.tet.2013.08.084

Reference yield:

: 78843-66-0,118110-66-0,137967-42-1
(S)-3-Phenyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-propionic acid ethyl ester

: 1462968-82-6
(S,Z)-N-(1-ethoxy-1-oxo-3-phenylpropan-2-yl)-2-methylpropan-1-imine oxide

Guidance literature:: Multi-step reaction with 3 steps

1: urea hydrogen peroxide adduct; magnesium sulfate; methyltrioxorhenium(VII) / methanol / 7 h / 20 °C

2: sodium hydroxide; acetic acid; hydroxylamine hydrochloride / methanol / 16 h / Reflux

3: magnesium sulfate / 4 h / 20 °C

With hydroxylamine hydrochloride; urea hydrogen peroxide adduct; methyltrioxorhenium(VII); magnesium sulfate; acetic acid; sodium hydroxide; In methanol;
DOI:10.1016/j.tet.2013.08.084