6-Chloro-2-(4-chloro-2-fluoro-3-methoxyphenyl)-5-methoxypyrimidin-4-ylamine

Base Information

• Chemical Name: 6-Chloro-2-(4-chloro-2-fluoro-3-methoxyphenyl)-5-methoxypyrimidin-4-ylamine
• CAS No.: 1126320-83-9
• Molecular Formula: C₁₂H₁₀Cl₂FN₃O₂
• Molecular Weight: 318.135

Synonyms:6-Chloro-2-(4-chloro-2-fluoro-3-methoxyphenyl)-5-methoxypyrimidin-4-ylamine

Chemical Property of 6-Chloro-2-(4-chloro-2-fluoro-3-methoxyphenyl)-5-methoxypyrimidin-4-ylamine

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Technology Process of 6-Chloro-2-(4-chloro-2-fluoro-3-methoxyphenyl)-5-methoxypyrimidin-4-ylamine

There total 1 articles about 6-Chloro-2-(4-chloro-2-fluoro-3-methoxyphenyl)-5-methoxypyrimidin-4-ylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

4,6-Dichloro-2-(4-chloro-2-fluoro-3-methoxyphenyl)-5-methoxypyrimidine (1126320-74-8) → 6-Chloro-2-(4-chloro-2-fluoro-3-methoxyphenyl)-5-methoxypyrimidin-4-ylamine (1126320-83-9)

Guidance literature:

With ammonia; In ethanol; at 125 ℃; for 0.5h; Microwave irradiation;

Reference yield: 47.0%

methanol (67-56-1) + 6-Chloro-2-(4-chloro-2-fluoro-3-methoxyphenyl)-5-methoxypyrimidin-4-ylamine (1126320-83-9) + carbon monoxide (201230-82-2) → methyl 6-amino-2-(4-chloro-2-fluoro-3-methoxyphenyl)-5-methoxypyrimidine-4-carboxylate (1126318-85-1)

Guidance literature:

With triethylamine; 1,4-di(diphenylphosphino)-butane; palladium diacetate; at 125 ℃; for 18h; under 15514.9 Torr;

upstream raw materials:

4,6-Dichloro-2-(4-chloro-2-fluoro-3-methoxyphenyl)-5-methoxypyrimidine

Downstream raw materials:

methyl 6-amino-2-(4-chloro-2-fluoro-3-methoxyphenyl)-5-methoxypyrimidine-4-carboxylate

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