C₂₇H₂₉F₂NO₃

Base Information

Chemical Name:C₂₇H₂₉F₂NO₃
CAS No.:1427407-94-0
Molecular Formula:C₂₇H₂₉F₂NO₃
Molecular Weight:453.529
Hs Code.:

C<sub>27</sub>H<sub>29</sub>F<sub>2</sub>NO<sub>3</sub>

Synonyms:C₂₇H₂₉F₂NO₃

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Chemical Property of C₂₇H₂₉F₂NO₃

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Technology Process of C₂₇H₂₉F₂NO₃

There total 11 articles about C₂₇H₂₉F₂NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 29921-57-1
isopropyl 2-bromoacetate

: 1427407-93-9
3-[[2-fluoro-5-(3-fluorophenyl)-3-methylphenyl]methylamino]-2,4-dimethylphenol

: 1427407-94-0
C₂₇H₂₉F₂NO₃

Guidance literature:: 3-[[2-fluoro-5-(3-fluorophenyl)-3-methylphenyl]methylamino]-2,4-dimethylphenol; With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

isopropyl 2-bromoacetate; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

Reference yield:

: 2198-53-0
N-(2,6-dimethylphenyl)acetamide

: 1427407-94-0
C₂₇H₂₉F₂NO₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: nitric acid; acetic acid; sulfuric acid / 1 h / 0 - 20 °C

2.1: palladium 10% on activated carbon; hydrogen / ethanol; methanol; acetic acid / 36 h / 20 °C

3.1: sodium nitrite; sulfuric acid / water / 0.5 h / 0 °C

3.2: 2 h / 100 °C

4.1: dmap; triethylamine / N,N-dimethyl-formamide / 50 °C

5.1: hydrazine hydrate / tert-butyl alcohol / 110 °C / Inert atmosphere

6.1: trifluoroacetic acid / dichloromethane / 20 °C

7.1: sodium hydrogencarbonate / tetrahydrofuran / 1 h / 0 - 20 °C

8.1: borane-THF / tetrahydrofuran / 60 °C / Inert atmosphere

9.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

9.2: 1 h / 20 °C

With dmap; borane-THF; sulfuric acid; palladium 10% on activated carbon; hydrogen; nitric acid; sodium hydrogencarbonate; caesium carbonate; hydrazine hydrate; acetic acid; triethylamine; trifluoroacetic acid; sodium nitrite; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 5416-12-6
N-(2,6-dimethyl-3-nitro-phenyl)acetamide

: 1427407-94-0
C₂₇H₂₉F₂NO₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: palladium 10% on activated carbon; hydrogen / ethanol; methanol; acetic acid / 36 h / 20 °C

2.1: sodium nitrite; sulfuric acid / water / 0.5 h / 0 °C

2.2: 2 h / 100 °C

3.1: dmap; triethylamine / N,N-dimethyl-formamide / 50 °C

4.1: hydrazine hydrate / tert-butyl alcohol / 110 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane / 20 °C

6.1: sodium hydrogencarbonate / tetrahydrofuran / 1 h / 0 - 20 °C

7.1: borane-THF / tetrahydrofuran / 60 °C / Inert atmosphere

8.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

8.2: 1 h / 20 °C

With dmap; borane-THF; sulfuric acid; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; caesium carbonate; hydrazine hydrate; triethylamine; trifluoroacetic acid; sodium nitrite; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; tert-butyl alcohol;