2,4,6,8,10,12,14-Heptaoxapentadecane

Base Information

• Chemical Name: 2,4,6,8,10,12,14-Heptaoxapentadecane
• CAS No.: 13352-77-7
• Molecular Formula: C8H18 O7
• Molecular Weight: 226.227
• DSSTox Substance ID: DTXSID30702969
• Nikkaji Number: J2.873.939G
• Wikidata: Q82635012
• Mol file: 13352-77-7.mol

Synonyms:Ether,bis[[(methoxymethoxy)methoxy]methyl]; Hexakis(oxymethylene)dimethyl ether

Chemical Property of 2,4,6,8,10,12,14-Heptaoxapentadecane

Chemical Property:

• Melting Point: 38℃
• Boiling Point: 154-165℃/8Torr
• PSA: 64.61000
• LogP: 0.10720
• XLogP3: -0.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 7
• Rotatable Bond Count: 12
• Exact Mass: 226.10525291
• Heavy Atom Count: 15
• Complexity: 99.2

Purity/Quality:

98.00% ^*data from raw suppliers

2,4,6,8,10,12,14-heptaoxapentadecane 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COCOCOCOCOCOCOC

Technology Process of 2,4,6,8,10,12,14-Heptaoxapentadecane

There total 9 articles about 2,4,6,8,10,12,14-Heptaoxapentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3,5-Trioxan (110-88-3) + 1,1-dimethoxyethane (534-15-6) → C11H24O10 + C13H28O12 + bis-methoxymethoxy-methane (13353-03-2) + bis(methoxymethyl)ether (628-90-0) + POMM4 (13352-75-5) + CH3-(OCH2)8-OCH3 (13352-78-8) + Methoxymethoxymethoxymethoxymethoxy-methoxymethoxymethoxymethoxymethoxymethoxy-methane (54261-86-8) + POMM5 (13352-76-6) + CH3-(OCH2)7-OCH3 (13353-04-3) + CH3-(OCH2)6-OCH3 (13352-77-7)

Guidance literature:

Amberlite IR 120; at 100 ℃; for 24h; Product distribution / selectivity;

Reference yield:

1,3,5-Trioxan (110-88-3) + 1,1-dimethoxyethane (534-15-6) + bis(methoxymethyl)ether (628-90-0) → C11H24O10 + C13H28O12 + bis-methoxymethoxy-methane (13353-03-2) + POMM4 (13352-75-5) + CH3-(OCH2)8-OCH3 (13352-78-8) + Methoxymethoxymethoxymethoxymethoxy-methoxymethoxymethoxymethoxymethoxymethoxy-methane (54261-86-8) + POMM5 (13352-76-6) + CH3-(OCH2)7-OCH3 (13353-04-3) + CH3-(OCH2)6-OCH3 (13352-77-7)

Guidance literature:

sulfuric acid; In water; at 100 ℃; for 12h; Product distribution / selectivity;

Reference yield:

1,3,5-Trioxan (110-88-3) + bis(methoxymethyl)ether (628-90-0) → C11H24O10 + C13H28O12 + 1,1-dimethoxyethane (534-15-6) + bis-methoxymethoxy-methane (13353-03-2) + POMM4 (13352-75-5) + CH3-(OCH2)8-OCH3 (13352-78-8) + Methoxymethoxymethoxymethoxymethoxy-methoxymethoxymethoxymethoxymethoxymethoxy-methane (54261-86-8) + POMM5 (13352-76-6) + CH3-(OCH2)7-OCH3 (13353-04-3) + CH3-(OCH2)6-OCH3 (13352-77-7)

Guidance literature:

sulfuric acid; In water; at 100 ℃; for 12h; Product distribution / selectivity;

upstream raw materials:

1,3,5-Trioxan

1,1-dimethoxyethane

bis(methoxymethyl)ether

formaldehyd

Downstream raw materials:

Bis(2-hydroxyphenyl)methane

2-[(4-hydroxyphenyl)methyl]phenol

bis-(4-hydroxyphenyl)methane

Refernces

• 1、 Wu, Qin,Li, Weijiao,Wang, Min,Hao, Yu,Chu, Tonghua,Shang, Jiqing,Li, Hansheng,Zhao, Yun,Jiao, Qingze. "Synthesis of polyoxymethylene dimethyl ethers from methylal and trioxane catalyzed by Br?nsted acid ionic liquids with different alkyl groups". . p. 57968 - 57974. Retrieved 2015/07/20.
• 2、 -. "PERFLOURINATED POLY(OXYMETHYLENE) COMPOUNDS". Page/Page column 20-21. . Retrieved 2010/07/10.