2,3-O-isopropylidene-5-O-(1-methoxy-1-methyl-ethyl)-D-ribono-1,4-lactone

Base Information

Chemical Name:2,3-O-isopropylidene-5-O-(1-methoxy-1-methyl-ethyl)-D-ribono-1,4-lactone
CAS No.:162635-53-2
Molecular Formula:C₁₂H₂₀O₆
Molecular Weight:260.287
Hs Code.:

Synonyms:2,3-O-isopropylidene-5-O-(1-methoxy-1-methyl-ethyl)-D-ribono-1,4-lactone

Suppliers and Price of 2,3-O-isopropylidene-5-O-(1-methoxy-1-methyl-ethyl)-D-ribono-1,4-lactone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 6 raw suppliers

Chemical Property of 2,3-O-isopropylidene-5-O-(1-methoxy-1-methyl-ethyl)-D-ribono-1,4-lactone

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 2,3-O-isopropylidene-5-O-(1-methoxy-1-methyl-ethyl)-D-ribono-1,4-lactone

There total 2 articles about 2,3-O-isopropylidene-5-O-(1-methoxy-1-methyl-ethyl)-D-ribono-1,4-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 77-76-9
2,2-dimethoxy-propane

: 5336-08-3
D-Ribono-1,4-lactone

: 30725-00-9
2,3-O-isopropylidene-D-ribonic-γ-lactone

: 162635-53-2
2,3-O-isopropylidene-5-O-(1-methoxy-1-methyl-ethyl)-D-ribono-1,4-lactone

: 188192-03-2
(3aR,7R,7aR)-7-(1-Methoxy-1-methyl-ethoxy)-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-4-one

Guidance literature:: With toluene-4-sulfonic acid; at 25 ℃; for 24h;
DOI:10.1016/S0040-4020(96)01079-4

Reference yield: 10.0%

: 116-11-0
2-Methoxypropene

: 5336-08-3
D-Ribono-1,4-lactone

: 30725-00-9
2,3-O-isopropylidene-D-ribonic-γ-lactone

: 162635-53-2
2,3-O-isopropylidene-5-O-(1-methoxy-1-methyl-ethyl)-D-ribono-1,4-lactone

Guidance literature:: With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; at 0 ℃; for 5h;
DOI:10.1016/0008-6215(94)00190-1

Reference yield: 91.0%

: 108-86-1,52753-63-6
bromobenzene

: 162635-53-2
2,3-O-isopropylidene-5-O-(1-methoxy-1-methyl-ethyl)-D-ribono-1,4-lactone

: 1224588-06-0
(3aR,6R,6aR)-6-(2-methoxypropan-2-yloxy)methyl-2,2-dimethyl-4-phenyltetrahydrofuro[3,4-d][1,3]dioxol-4-ol

Guidance literature:: bromobenzene; With tert.-butyl lithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

2,3-O-isopropylidene-5-O-(1-methoxy-1-methyl-ethyl)-D-ribono-1,4-lactone; In tetrahydrofuran; hexane; at -78 ℃; for 1.5h;

With water; sodium chloride; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1016/j.tet.2010.01.107