N-{5-[4-(3-chloropropoxy)benzamido]-2-methylphenyl}-3,4-dimethoxybenzamide

Base Information

• Chemical Name: N-{5-[4-(3-chloropropoxy)benzamido]-2-methylphenyl}-3,4-dimethoxybenzamide
• CAS No.: 250679-75-5
• Molecular Formula: C₂₆H₂₇ClN₂O₅
• Molecular Weight: 482.964

Synonyms:N-{5-[4-(3-chloropropoxy)benzamido]-2-methylphenyl}-3,4-dimethoxybenzamide

Chemical Property of N-{5-[4-(3-chloropropoxy)benzamido]-2-methylphenyl}-3,4-dimethoxybenzamide

Chemical Property:

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Technology Process of N-{5-[4-(3-chloropropoxy)benzamido]-2-methylphenyl}-3,4-dimethoxybenzamide

There total 1 articles about N-{5-[4-(3-chloropropoxy)benzamido]-2-methylphenyl}-3,4-dimethoxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

oxalyl dichloride (79-37-8) + N-(5-amino-2-methylphenyl)-3,4-dimethoxybenzamide (221875-97-4) + 4-(3-chloropropoxy)benzoic acid (65136-52-9) → N-{5-[4-(3-chloropropoxy)benzamido]-2-methylphenyl}-3,4-dimethoxybenzamide (250679-75-5)

Guidance literature:

With pyridine; In hydrogenchloride; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

morpholine (110-91-8,99108-56-2) + N-{5-[4-(3-chloropropoxy)benzamido]-2-methylphenyl}-3,4-dimethoxybenzamide (250679-75-5) → N-{2-methyl-5-[4-(3-morpholinopropoxy)benzamido]phenyl}-3,4-dimethoxybenzamide (250679-79-9)

Guidance literature:

With sodium iodide; In acetone;

Reference yield:

N-{5-[4-(3-chloropropoxy)benzamido]-2-methylphenyl}-3,4-dimethoxybenzamide (250679-75-5) + S,S-Dioxothiamorpholine trifluoroacetic acid salt + N-ethyl-N,N-diisopropylamine (7087-68-5) → N-{5-[4-(3-hydroxypropoxy)benzamido]-2-methylphenyl}-3,4-dimethoxybenzamide (250680-54-7)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; 2,4-dichlorophenoxyacetic acid dimethylamine;

upstream raw materials:

oxalyl dichloride

N-(5-amino-2-methylphenyl)-3,4-dimethoxybenzamide

4-(3-chloropropoxy)benzoic acid

Downstream raw materials:

N-{2-methyl-5-[4-(3-morpholinopropoxy)benzamido]phenyl}-3,4-dimethoxybenzamide

N-{5-[4-(3-hydroxypropoxy)benzamido]-2-methylphenyl}-3,4-dimethoxybenzamide

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