2-{[2-(4-methoxyphenyl)-1H-benzimidazol-1-yl]acetyl}-N-methylhydrazinecarbothioamide

Base Information

Chemical Name:2-{[2-(4-methoxyphenyl)-1H-benzimidazol-1-yl]acetyl}-N-methylhydrazinecarbothioamide
CAS No.:1029062-45-0
Molecular Formula:C₁₈H₁₉N₅O₂S
Molecular Weight:369.447
Hs Code.:

Synonyms:2-{[2-(4-methoxyphenyl)-1H-benzimidazol-1-yl]acetyl}-N-methylhydrazinecarbothioamide

Suppliers and Price of 2-{[2-(4-methoxyphenyl)-1H-benzimidazol-1-yl]acetyl}-N-methylhydrazinecarbothioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-{[2-(4-methoxyphenyl)-1H-benzimidazol-1-yl]acetyl}-N-methylhydrazinecarbothioamide

Chemical Property:

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Technology Process of 2-{[2-(4-methoxyphenyl)-1H-benzimidazol-1-yl]acetyl}-N-methylhydrazinecarbothioamide

There total 5 articles about 2-{[2-(4-methoxyphenyl)-1H-benzimidazol-1-yl]acetyl}-N-methylhydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 477542-78-2
[2-(4-methoxyphenyl)-1H-benzimidazol-1-yl]-acetic acid hydrazide

: 556-61-6
methyl thioisocyanate

: 1029062-45-0
2-{[2-(4-methoxyphenyl)-1H-benzimidazol-1-yl]acetyl}-N-methylhydrazinecarbothioamide

Guidance literature:: In ethanol; for 3h; Reflux;
DOI:10.1016/j.ejmech.2019.04.012

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1029062-45-0
2-{[2-(4-methoxyphenyl)-1H-benzimidazol-1-yl]acetyl}-N-methylhydrazinecarbothioamide

Guidance literature:: Multi-step reaction with 4 steps

1: sodium metabisulfite

2: potassium hydroxide / dimethyl sulfoxide

3: hydrazine hydrate / ethanol

4: ethanol / 3 h / Reflux

With sodium metabisulfite; hydrazine hydrate; potassium hydroxide; In ethanol; dimethyl sulfoxide;
DOI:10.1016/j.ejmech.2019.04.012

Reference yield:

: 2620-81-7
2-(4-methoxyphenyl)-1H-benzimidazole

: 1029062-45-0
2-{[2-(4-methoxyphenyl)-1H-benzimidazol-1-yl]acetyl}-N-methylhydrazinecarbothioamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / dimethyl sulfoxide

2: hydrazine hydrate / ethanol

3: ethanol / 3 h / Reflux

With hydrazine hydrate; potassium hydroxide; In ethanol; dimethyl sulfoxide;
DOI:10.1016/j.ejmech.2019.04.012