10-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

Base Information

Chemical Name:10-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine
CAS No.:1333324-92-7
Molecular Formula:C₂₄H₂₄BNO₂S
Molecular Weight:401.337
Hs Code.:

Synonyms:10-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 10-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

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Technology Process of 10-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

There total 7 articles about 10-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 89922-57-6
3-bromo-10-phenylphenothiazine

: 73183-34-3
bis(pinacol)diborane

: 1333324-92-7
10-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In toluene; for 16h; Reflux;

Reference yield: 80.0%

: 1392069-86-1
3-iodo-10-phenyl-10H-phenothiazine

: 73183-34-3
bis(pinacol)diborane

: 1333324-92-7
10-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

Guidance literature:: With [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); potassium acetate; In dimethyl sulfoxide; at 80 ℃; for 1h; Inert atmosphere;
DOI:10.1007/s11164-012-0642-6

Reference yield:

: 18073-95-5
3-amino-10-phenyl-10H-phenothiazine

: 1333324-92-7
10-phenyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-10H-phenothiazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 0.67 h / 0 °C / Inert atmosphere

1.2: 1 h / 0 °C / Inert atmosphere

1.3: 20 h / 20 °C / Inert atmosphere

2.1: methyl iodide; iodine / toluene / 2 h / 55 °C / Inert atmosphere; Sealed tube

3.1: [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); potassium acetate / dimethyl sulfoxide / 1 h / 80 °C / Inert atmosphere

With [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); boron trifluoride diethyl etherate; iodine; potassium acetate; methyl iodide; In dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1007/s11164-012-0642-6