Methyl (S)-{4-(4-chlorophenyl)-2-(tert-butyldimethylsilyloxymethyl)-3,9-dimethyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepin-6-yl}acetate

Base Information

Chemical Name:Methyl (S)-{4-(4-chlorophenyl)-2-(tert-butyldimethylsilyloxymethyl)-3,9-dimethyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepin-6-yl}acetate
CAS No.:916493-50-0
Molecular Formula:C₂₆H₃₃ClN₄O₃SSi
Molecular Weight:545.178
Hs Code.:

Synonyms:Methyl (S)-{4-(4-chlorophenyl)-2-(tert-butyldimethylsilyloxymethyl)-3,9-dimethyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepin-6-yl}acetate

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Chemical Property of Methyl (S)-{4-(4-chlorophenyl)-2-(tert-butyldimethylsilyloxymethyl)-3,9-dimethyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepin-6-yl}acetate

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Technology Process of Methyl (S)-{4-(4-chlorophenyl)-2-(tert-butyldimethylsilyloxymethyl)-3,9-dimethyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepin-6-yl}acetate

There total 1 articles about Methyl (S)-{4-(4-chlorophenyl)-2-(tert-butyldimethylsilyloxymethyl)-3,9-dimethyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepin-6-yl}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 916491-91-3
methyl [(6S)-4-(4-chlorophenyl)-2-(hydroxymethyl)-3,9-dimethyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepin-6-yl]acetate

: 18162-48-6
tert-butyldimethylsilyl chloride

: 916493-50-0
Methyl (S)-{4-(4-chlorophenyl)-2-(tert-butyldimethylsilyloxymethyl)-3,9-dimethyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepin-6-yl}acetate

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

Reference yield:

: 67-56-1
methanol

: 916493-50-0
Methyl (S)-{4-(4-chlorophenyl)-2-(tert-butyldimethylsilyloxymethyl)-3,9-dimethyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepin-6-yl}acetate

: 124-41-4
sodium methylate

: 150255-96-2
(3‐cyanophenyl)boronic acid

: Methyl (S)-{4-(3'-cyanobiphenyl-4-yl)-2-methoxymethyl-3,9-dimethyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepin-6-yl}acetate

Guidance literature:: Methyl (S)-{4-(4-chlorophenyl)-2-(tert-butyldimethylsilyloxymethyl)-3,9-dimethyl-6H-thieno[3,2-f][1,2,4]triazolo[4,3-a][1,4]diazepin-6-yl}acetate; (3‐cyanophenyl)boronic acid; With potassium fluoride; palladium diacetate; johnphos; In tetrahydrofuran; for 8h; Heating / reflux;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h;

methanol; sodium methylate; With methanesulfonyl chloride; triethylamine; more than 3 stages;