methyl-3-<4-methoxy-<3-<4-(2-(hydroxymethyl)ethynyl)phenoxy>phenyl>>propanoate

Base Information

Chemical Name:methyl-3-<4-methoxy-<3-<4-(2-(hydroxymethyl)ethynyl)phenoxy>phenyl>>propanoate
CAS No.:143551-92-2
Molecular Formula:C₂₀H₂₀O₅
Molecular Weight:340.376
Hs Code.:

Synonyms:methyl-3-<4-methoxy-<3-<4-(2-(hydroxymethyl)ethynyl)phenoxy>phenyl>>propanoate

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Chemical Property of methyl-3-<4-methoxy-<3-<4-(2-(hydroxymethyl)ethynyl)phenoxy>phenyl>>propanoate

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Technology Process of methyl-3-<4-methoxy-<3-<4-(2-(hydroxymethyl)ethynyl)phenoxy>phenyl>>propanoate

There total 15 articles about methyl-3-<4-methoxy-<3-<4-(2-(hydroxymethyl)ethynyl)phenoxy>phenyl>>propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 67-56-1
methanol

: 176659-16-8
(E) ethyl 4-methoxy-3-<4-(2-(hydroxymethyl)ethynyl)phenoxy> cinnamate

: 143551-92-2
methyl-3-<4-methoxy-<3-<4-(2-(hydroxymethyl)ethynyl)phenoxy>phenyl>>propanoate

Guidance literature:: With magnesium; at 10 ℃; for 2.5h;
DOI:10.1080/00397919608003541

Reference yield: 56.0%

: 107-19-7
propargyl alcohol

: 143551-91-1
3-[3-(4-Iodo-phenoxy)-4-methoxy-phenyl]-propionic acid methyl ester

: 143551-92-2
methyl-3-<4-methoxy-<3-<4-(2-(hydroxymethyl)ethynyl)phenoxy>phenyl>>propanoate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine;
DOI:10.1016/S0040-4039(00)74692-2

Reference yield:

: 100-00-5
4-chlorobenzonitrile

: 143551-92-2
methyl-3-<4-methoxy-<3-<4-(2-(hydroxymethyl)ethynyl)phenoxy>phenyl>>propanoate

Guidance literature:: Multi-step reaction with 7 steps

2: 80 percent / pyridine, piperidine

3: 85 percent / H₂ / 10 percent Pd/C

4: H₂SO₄, NaNO₂ / 5 °C

5: KI

6: 96 percent / K₂CO₃ / acetone

7: 56 percent / (PPh₃)2PdCl₂, CuI, Et₃N

With piperidine; pyridine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sulfuric acid; hydrogen; potassium carbonate; triethylamine; potassium iodide; sodium nitrite; palladium on activated charcoal; In acetone;
DOI:10.1016/S0040-4039(00)74692-2