N'-phenylhydrazine carboxylic acid 1-propylbutyl ester

Base Information

Chemical Name:N'-phenylhydrazine carboxylic acid 1-propylbutyl ester
CAS No.:40887-25-0
Molecular Formula:C₁₄H₂₂N₂O₂
Molecular Weight:250.341
Hs Code.:

Synonyms:N'-phenylhydrazine carboxylic acid 1-propylbutyl ester

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Chemical Property of N'-phenylhydrazine carboxylic acid 1-propylbutyl ester

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Technology Process of N'-phenylhydrazine carboxylic acid 1-propylbutyl ester

There total 3 articles about N'-phenylhydrazine carboxylic acid 1-propylbutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 998-93-6
4-bromoheptane

: 124-38-9,18923-20-1
carbon dioxide

: 100-63-0
phenylhydrazine

: 40887-25-0
N'-phenylhydrazine carboxylic acid 1-propylbutyl ester

Guidance literature:: carbon dioxide; phenylhydrazine; In dimethyl sulfoxide; at 60 ℃; for 0.5h; Inert atmosphere;

With N-benzyl-trimethylammonium hydroxide; In dimethyl sulfoxide; at 60 ℃; for 0.5h; Inert atmosphere;

4-bromoheptane; In dimethyl sulfoxide; at 60 ℃; Inert atmosphere;
DOI:10.1007/s00706-008-0955-8

Reference yield: 86.0%

: 124-38-9,18923-20-1
carbon dioxide

: 4883-86-7
4-heptyltoluene-p-sulphonate

: 100-63-0
phenylhydrazine

: 40887-25-0
N'-phenylhydrazine carboxylic acid 1-propylbutyl ester

Guidance literature:: carbon dioxide; phenylhydrazine; With N-benzyl-trimethylammonium hydroxide; In dimethyl sulfoxide; at 60 ℃; for 0.5h; Inert atmosphere;

4-heptyltoluene-p-sulphonate; In dimethyl sulfoxide; at 60 ℃; for 4.5h; Inert atmosphere;
DOI:10.1080/00397910802269259

Reference yield: 86.0%

: 589-55-9
heptan-4-ol

: 124-38-9,18923-20-1
carbon dioxide

: 100-63-0
phenylhydrazine

: 40887-25-0
N'-phenylhydrazine carboxylic acid 1-propylbutyl ester

Guidance literature:: carbon dioxide; phenylhydrazine; In dimethyl sulfoxide; at 20 ℃; for 0.5h; Inert atmosphere;

heptan-4-ol; With triphenylphosphine; diethylazodicarboxylate; In dimethyl sulfoxide; at 20 ℃; for 2.5h; chemoselective reaction; Inert atmosphere;
DOI:10.1007/BF03249073