N-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranuronosyl)amide-isophthalamic acid

Base Information

Chemical Name:N-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranuronosyl)amide-isophthalamic acid
CAS No.:755023-81-5
Molecular Formula:C₂₁H₂₃NO₁₂
Molecular Weight:481.413
Hs Code.:

Synonyms:N-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranuronosyl)amide-isophthalamic acid

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Chemical Property of N-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranuronosyl)amide-isophthalamic acid

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Technology Process of N-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranuronosyl)amide-isophthalamic acid

There total 2 articles about N-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranuronosyl)amide-isophthalamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 14365-73-2
2,3,4-tri-O-acetyl-β-D-glucopyranosylamine uronic acid methyl ester

: 121-91-5
isophthalic acid

: 755023-81-5
N-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranuronosyl)amide-isophthalamic acid

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In N,N-dimethyl-formamide; for 24h;
DOI:10.1016/j.carres.2004.05.024

Reference yield:

: 67776-38-9,163776-36-1
2,3,4-tri-O-acetyl-1-azido-1-deoxy-β-D-glucopyranuronic acid methyl ester

: 755023-81-5
N-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranuronosyl)amide-isophthalamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / tetrahydrofuran / -5 °C

2: 41 percent / HOBt; EDC; Et₃N / dimethylformamide / 24 h

With hydrogen; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; palladium on activated charcoal; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2004.05.024

Reference yield: 28.0%

: 462-94-2
1,5-diaminopentane

: 755023-81-5
N-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranuronosyl)amide-isophthalamic acid

: 755023-88-2
C₄₇H₅₆N₄O₂₂

Guidance literature:: With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃; for 19h;
DOI:10.1016/j.carres.2004.05.024