1-<2-(4-fluorophenyl)-4,4-dicarbomethoxycyclopenten-1-yl>-4-(methylsulfonyl)benzene

Base Information

• Chemical Name: 1-<2-(4-fluorophenyl)-4,4-dicarbomethoxycyclopenten-1-yl>-4-(methylsulfonyl)benzene
• CAS No.: 159429-83-1
• Molecular Formula: C₂₂H₂₁FO₆S
• Molecular Weight: 432.47

Synonyms:1-<2-(4-fluorophenyl)-4,4-dicarbomethoxycyclopenten-1-yl>-4-(methylsulfonyl)benzene

Chemical Property of 1-<2-(4-fluorophenyl)-4,4-dicarbomethoxycyclopenten-1-yl>-4-(methylsulfonyl)benzene

Chemical Property:

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Technology Process of 1-<2-(4-fluorophenyl)-4,4-dicarbomethoxycyclopenten-1-yl>-4-(methylsulfonyl)benzene

There total 18 articles about 1-<2-(4-fluorophenyl)-4,4-dicarbomethoxycyclopenten-1-yl>-4-(methylsulfonyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

2-(4-fluorophenyl)-3-<4-(methylsulfonyl)phenyl>-1,4-dichloro-2-butene + malonic acid dimethyl ester (108-59-8) → 1-<2-(4-fluorophenyl)-4,4-dicarbomethoxycyclopenten-1-yl>-4-(methylsulfonyl)benzene (159429-83-1)

Guidance literature:

With lithium hydride; In N,N-dimethyl-formamide; for 19h;

DOI:10.1021/jm950664x

Reference yield:

dimethyl 2-[2-(4-fluorophenyl)-2-oxoethyl]-2-[2-[4-(methylsulfonyl)phenyl]-2-oxoethyl]propanedioate (159429-82-0) → 1-<2-(4-fluorophenyl)-4,4-dicarbomethoxycyclopenten-1-yl>-4-(methylsulfonyl)benzene (159429-83-1)

Guidance literature:

With titanium tetrachloride; zinc; In tetrahydrofuran;

DOI:10.1021/jm00049a005

Reference yield:

titanium tetrachloride (7550-45-0) + dimethyl 2-[2-(4-fluorophenyl)-2-oxoethyl]-2-[2-[4-(methylsulfonyl)phenyl]-2-oxoethyl]propanedioate (159429-82-0) → 1-<2-(4-fluorophenyl)-4,4-dicarbomethoxycyclopenten-1-yl>-4-(methylsulfonyl)benzene (159429-83-1)

Guidance literature:

With zinc; In tetrahydrofuran;

upstream raw materials:

dimethyl 2-[2-(4-fluorophenyl)-2-oxoethyl]-2-[2-[4-(methylsulfonyl)phenyl]-2-oxoethyl]propanedioate

malonic acid dimethyl ester

2-bromo-1-(4-methanesulfonylphenyl)ethanone

4-(Methylthio)acetophenone

Downstream raw materials:

1-<2-(4-fluorophenyl)-4,4-bis(hydroxymethyl)cyclopenten-1-yl>-4-(methylsulfonl)benzene

4-[6-(4-fluorophenyl)spiro[2.4]hept-5-en-5-yl]benzenesulfonamide

SC-58451

1-<2-(4-fluorophenyl)-4,4-bis(tosylmethyl)cyclopenten-1-yl>-4-(methylsulfonyl)benzene

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