Technology Process of C10H11ClN2O
There total 4 articles about C10H11ClN2O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 20 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dimethylsulfide borane complex / hexane / 2 h / Reflux; Inert atmosphere
2: potassium acetate / tetrahydrofuran; water / 2 h / 20 °C
3: triethylamine / dichloromethane / 0.17 h / 0 °C
4: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C
With
dimethylsulfide borane complex; potassium acetate; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; hexane; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium acetate / tetrahydrofuran; water / 2 h / 20 °C
2: triethylamine / dichloromethane / 0.17 h / 0 °C
3: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C
With
potassium acetate; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; water;