N,N'-bis(trimethylsilyl)benzamidinate aluminum dichloride

Base Information

Chemical Name:N,N'-bis(trimethylsilyl)benzamidinate aluminum dichloride
CAS No.:120140-60-5
Molecular Formula:C₁₃H₂₃AlCl₂N₂Si₂
Molecular Weight:361.398
Hs Code.:

Synonyms:N,N'-bis(trimethylsilyl)benzamidinate aluminum dichloride

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Chemical Property of N,N'-bis(trimethylsilyl)benzamidinate aluminum dichloride

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Technology Process of N,N'-bis(trimethylsilyl)benzamidinate aluminum dichloride

There total 3 articles about N,N'-bis(trimethylsilyl)benzamidinate aluminum dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 7446-70-0
aluminium trichloride

: 24261-90-3
N,N,N'-tris(trimethylsilyl)benzamidine

: 120140-60-5
N,N'-bis(trimethylsilyl)benzamidinate aluminum dichloride

Guidance literature:: In dichloromethane; byproducts: ClSi(CH3)3; addn. of soln. of org. compd. in CH2Cl2 to suspn. of AlCl3 in CH2Cl2 (stirring, room temp.), stirring (30 min); partial evapn., cooling (3 d, -28°C), filtn., washing (cold CH2Cl2), drying (vac.); elem. anal;

Reference yield: 58.0%

: 7446-70-0
aluminium trichloride

: lithium N,N'-bis(trimethylsilyl)benzamidinate

: 120140-60-5
N,N'-bis(trimethylsilyl)benzamidinate aluminum dichloride

Guidance literature:: In toluene; byproducts: LiCl; under inert conditions; Li compd. dissolved in dry toluene; cooled to -78°C; AlCl3 in dry toluene added dropwise; warmed to room temp.; stirred for 24 h; filtered through fritted glass; concd. by vac.; solid crystd. from toluene-hexane at -40°C; filtered; crystals dried under vac.; elem. anal.;
DOI:10.1021/om0602198