N-{tris[(2-tert-butoxycarbonyl)ethyl]methyl}-5-nitroisophthalimide monocarboxylic acid

Base Information

Chemical Name:N-{tris[(2-tert-butoxycarbonyl)ethyl]methyl}-5-nitroisophthalimide monocarboxylic acid
CAS No.:209679-61-8
Molecular Formula:C₃₀H₄₄N₂O₁₁
Molecular Weight:608.686
Hs Code.:

Synonyms:N-{tris[(2-tert-butoxycarbonyl)ethyl]methyl}-5-nitroisophthalimide monocarboxylic acid

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Chemical Property of N-{tris[(2-tert-butoxycarbonyl)ethyl]methyl}-5-nitroisophthalimide monocarboxylic acid

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Technology Process of N-{tris[(2-tert-butoxycarbonyl)ethyl]methyl}-5-nitroisophthalimide monocarboxylic acid

There total 1 articles about N-{tris[(2-tert-butoxycarbonyl)ethyl]methyl}-5-nitroisophthalimide monocarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 73585-90-7
5-nitroisophthalic monoacyl chloride

: 136586-99-7
4-amino-4-(2-tert-butoxycarbonylethyl)heptanedioic acid di-tertbutyl ester

: 209679-61-8
N-{tris[(2-tert-butoxycarbonyl)ethyl]methyl}-5-nitroisophthalimide monocarboxylic acid

Guidance literature:: With triethylamine; In tetrahydrofuran; at -5 ℃; for 12h;
DOI:10.1021/ja001401h

Reference yield: 84.0%

: 194213-77-9
5-([2,2':6',2''-terpyridin]-4'-yloxy)pentan-1-amine

: 209679-61-8
N-{tris[(2-tert-butoxycarbonyl)ethyl]methyl}-5-nitroisophthalimide monocarboxylic acid

: 209679-62-9
N-{tris[(2-tert-butoxycarbonyl)ethyl]methyl}-N'-[4'-oxa-(2,2':6',2''-terpyridinyl)]-5-nitroisophthalimide

Guidance literature:: N-{tris[(2-tert-butoxycarbonyl)ethyl]methyl}-5-nitroisophthalimide monocarboxylic acid; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 25 ℃; for 1h;

5-([2,2':6',2''-terpyridin]-4'-yloxy)pentan-1-amine; In N,N-dimethyl-formamide; Further stages.;
DOI:10.1021/ja001401h

Reference yield:

: 209679-61-8
N-{tris[(2-tert-butoxycarbonyl)ethyl]methyl}-5-nitroisophthalimide monocarboxylic acid

: 4-{3-amino-5-[5-([2,2';6',2'']terpyridin-4'-yloxy)-pentylcarbamoyl]-benzoylamino}-4-(2-tert-butoxycarbonyl-ethyl)-heptanedioic acid di-tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: dicyclohexylcarbodiimide; 1-hydroxybenzotriazole / dimethylformamide / 1 h / 25 °C

1.2: 84 percent / dimethylformamide

2.1: 87 percent / HCO₂NH₄ / 10percent Pd/C / methanol / 0.5 h / 50 °C

With ammonium formate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; 10percent Pd/C; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja001401h