5-nitroisophthalic monoacyl chloride

Base Information

• Chemical Name: 5-nitroisophthalic monoacyl chloride
• CAS No.: 73585-90-7
• Molecular Formula: C₈H₄ClNO₅
• Molecular Weight: 229.576

Synonyms:5-nitroisophthalic monoacyl chloride

Chemical Property of 5-nitroisophthalic monoacyl chloride

Chemical Property:

Purity/Quality:

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Technology Process of 5-nitroisophthalic monoacyl chloride

There total 2 articles about 5-nitroisophthalic monoacyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-nitro-1,3-benzenedicarbonylchloride (13438-30-7) → 5-nitroisophthalic monoacyl chloride (73585-90-7)

Guidance literature:

With phosphoric acid tributyl ester; water; at 20 ℃; for 6.66667h;

Reference yield:

5-nitrobenzene-1,3-dicarboxylic acid (618-88-2) → 5-nitroisophthalic monoacyl chloride (73585-90-7)

Guidance literature:

With phosphorus pentachloride;

DOI:10.1084/jem.67.5.709

Reference yield: 58.0%

5-nitroisophthalic monoacyl chloride (73585-90-7) + di-tert-butyl 4-amino-4-methylheptanedicarboxylate (220593-28-2) → 4-(3-carboxy-5-nitro-benzoylamino)-4-methyl-heptanedioic acid di-tert-butyl ester (220593-29-3)

Guidance literature:

With triethylamine; In tetrahydrofuran; at -5 ℃; for 12h;

DOI:10.1039/a806509h DOI:10.1021/ja001401h

upstream raw materials:

5-nitrobenzene-1,3-dicarboxylic acid

5-nitro-1,3-benzenedicarbonylchloride

Downstream raw materials:

4-(3-carboxy-5-nitro-benzoylamino)-4-methyl-heptanedioic acid di-tert-butyl ester

N-{tris[(2-tert-butoxycarbonyl)ethyl]methyl}-5-nitroisophthalimide monocarboxylic acid

4-(2-carboxy-ethyl)-4-{3-nitro-5-[5-([2,2';6',2'']terpyridin-4'-yloxy)-pentylcarbamoyl]-benzoylamino}-heptanedioic acid

N-{tris[(2-tert-butoxycarbonyl)ethyl]methyl}-N'-[4'-oxa-(2,2':6',2''-terpyridinyl)]-5-nitroisophthalimide

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