3-(2'-methylphenyl)-(Z)-propenoic acid methyl ester

Base Information Edit

Chemical Name:3-(2'-methylphenyl)-(Z)-propenoic acid methyl ester
CAS No.:75950-75-3
Molecular Formula:C₁₁H₁₂O₂
Molecular Weight:176.215
Hs Code.:
Mol file:75950-75-3.mol

Synonyms:3-(2'-methylphenyl)-(Z)-propenoic acid methyl ester

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Chemical Property of 3-(2'-methylphenyl)-(Z)-propenoic acid methyl ester Edit

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Technology Process of 3-(2'-methylphenyl)-(Z)-propenoic acid methyl ester

There total 57 articles about 3-(2'-methylphenyl)-(Z)-propenoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 5927-18-4
trimethyl phosphonoacetate

: 529-20-4
2-methylphenyl aldehyde

: 70625-62-6,75950-75-3,130451-86-4
methyl (E)-3-(2-methylphenyl)-2-propenoate

Guidance literature:: trimethyl phosphonoacetate; With sodium hydride; In tetrahydrofuran; paraffin oil; at 0 - 20 ℃; for 0.5h; Inert atmosphere;

2-methylphenyl aldehyde; In tetrahydrofuran; paraffin oil; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.202100026

Reference yield: 99.0%

: 615-37-2
ortho-methylphenyl iodide

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 70625-62-6,75950-75-3,130451-86-4
methyl (E)-3-(2-methylphenyl)-2-propenoate

Guidance literature:: With trihexyl(tetradecyl)phosphonium chloride; sodium acetate; palladium diacetate; In water; at 50 ℃; for 2h;
DOI:10.1016/j.tetlet.2004.08.103

Reference yield: 98.0%

: 67-56-1
methanol

: 93614-78-9,4549-82-0
3-(2-methylphenyl)prop-2-en-1-al

: 75950-75-3,130451-86-4,70625-62-6
3-(2-methylphenyl)acrylic acid methyl ester

Guidance literature:: With 3,5,3',5'-tetra-tert-butyl-4,4'-diphenoquinone; C₂₃H₁₉Cl₃N₃⁽¹⁺⁾*Cl^(1-); benzoic acid; In tetrahydrofuran; at 20 ℃; for 5h;
DOI:10.1002/anie.202104712