α-Methylene-4-nitrobenzeneacetic acid methyl ester

Base Information Edit

Chemical Name:α-Methylene-4-nitrobenzeneacetic acid methyl ester
CAS No.:28042-27-5
Molecular Formula:C₁₀H₉NO₄
Molecular Weight:207.186
Hs Code.:
Mol file:28042-27-5.mol

Synonyms:α-Methylene-4-nitrobenzeneacetic acid methyl ester

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Chemical Property of α-Methylene-4-nitrobenzeneacetic acid methyl ester Edit

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Technology Process of α-Methylene-4-nitrobenzeneacetic acid methyl ester

There total 11 articles about α-Methylene-4-nitrobenzeneacetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 67-56-1
methanol

: 51747-44-5
α-(p-nitrophenyl)acrylic acid

: 28042-27-5
α-Methylene-4-nitrobenzeneacetic acid methyl ester

Guidance literature:: With sulfuric acid;
DOI:10.1002/hlca.19860690828

Reference yield: 76.0%

: 636-98-6
p-nitrobenzene iodide

: 124582-37-2
methyl 2-(tributylstannanyl)-2-propenoate

: 28042-27-5
α-Methylene-4-nitrobenzeneacetic acid methyl ester

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; for 12h; Ambient temperature;
DOI:10.1016/S0040-4039(00)73712-9