2-((5-chloro-2-((3-nitrophenyl)amino)pyrimidin-4-yl)amino)-N-methylbenzenesulfonamide

Base Information

Chemical Name:2-((5-chloro-2-((3-nitrophenyl)amino)pyrimidin-4-yl)amino)-N-methylbenzenesulfonamide
CAS No.:1346447-82-2
Molecular Formula:C₁₇H₁₅ClN₆O₄S
Molecular Weight:434.863
Hs Code.:

Synonyms:2-((5-chloro-2-((3-nitrophenyl)amino)pyrimidin-4-yl)amino)-N-methylbenzenesulfonamide

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Chemical Property of 2-((5-chloro-2-((3-nitrophenyl)amino)pyrimidin-4-yl)amino)-N-methylbenzenesulfonamide

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Technology Process of 2-((5-chloro-2-((3-nitrophenyl)amino)pyrimidin-4-yl)amino)-N-methylbenzenesulfonamide

There total 4 articles about 2-((5-chloro-2-((3-nitrophenyl)amino)pyrimidin-4-yl)amino)-N-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 761440-11-3
2-((2-amino-5-chloropyrimidin-4-yl)amino)-N-methylbenzenesulfonamide

: 99-09-2
3-nitro-aniline

: 1346447-82-2
2-((5-chloro-2-((3-nitrophenyl)amino)pyrimidin-4-yl)amino)-N-methylbenzenesulfonamide

Guidance literature:: With toluene-4-sulfonic acid; In isopropyl alcohol; at 80 ℃; for 5h;

Reference yield:

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 1346447-82-2
2-((5-chloro-2-((3-nitrophenyl)amino)pyrimidin-4-yl)amino)-N-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane; methanol / 0.67 h / 0 - 20 °C

2: hydrogen / palladium 10% on activated carbon / methanol / 6 h / 20 °C

3: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

4: toluene-4-sulfonic acid / isopropyl alcohol / 5 h / 80 °C

With hydrogen; potassium carbonate; toluene-4-sulfonic acid; triethylamine; palladium 10% on activated carbon; In methanol; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 23530-40-7
N-methyl-2-nitrobenzenesulfonamide

: 1346447-82-2
2-((5-chloro-2-((3-nitrophenyl)amino)pyrimidin-4-yl)amino)-N-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 6 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

3: toluene-4-sulfonic acid / isopropyl alcohol / 5 h / 80 °C

With hydrogen; potassium carbonate; toluene-4-sulfonic acid; palladium 10% on activated carbon; In methanol; N,N-dimethyl-formamide; isopropyl alcohol;