6-amidino-2-naphthyl ε-benzyloxycarbonylaminocaproate methanesulfonate

Base Information

Chemical Name:6-amidino-2-naphthyl ε-benzyloxycarbonylaminocaproate methanesulfonate
CAS No.:84729-86-2
Molecular Formula:CH₄O₃S*C₂₅H₂₇N₃O₄
Molecular Weight:529.614
Hs Code.:

Synonyms:6-amidino-2-naphthyl ε-benzyloxycarbonylaminocaproate methanesulfonate

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Chemical Property of 6-amidino-2-naphthyl ε-benzyloxycarbonylaminocaproate methanesulfonate

Chemical Property:

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Technology Process of 6-amidino-2-naphthyl ε-benzyloxycarbonylaminocaproate methanesulfonate

There total 5 articles about 6-amidino-2-naphthyl ε-benzyloxycarbonylaminocaproate methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58200-88-7
6-Amidino-2-naphthol

: 84729-86-2
6-amidino-2-naphthyl ε-benzyloxycarbonylaminocaproate methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol

2: 1.) dicyclohexylcarbodiimide (DCC) / 1.) pyridine, room temp.; 2.) H₂O

With dicyclohexyl-carbodiimide; In methanol;
DOI:10.1248/cpb.33.1458

Reference yield:

: 15231-91-1
6-bromo-naphthalen-2-ol

: 84729-86-2
6-amidino-2-naphthyl ε-benzyloxycarbonylaminocaproate methanesulfonate

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / CuCN / dimethylformamide / 3 h / 160 - 170 °C

2: HCl / Ambient temperature

3: NH₃ / methanol / 3 h / 50 °C

4: methanol

5: 1.) dicyclohexylcarbodiimide (DCC) / 1.) pyridine, room temp.; 2.) H₂O

With hydrogenchloride; ammonia; dicyclohexyl-carbodiimide; In methanol; N,N-dimethyl-formamide;
DOI:10.1248/cpb.33.1458

Reference yield:

: 52927-22-7
6-cyano-2-naphthol

: 84729-86-2
6-amidino-2-naphthyl ε-benzyloxycarbonylaminocaproate methanesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: HCl / Ambient temperature

2: NH₃ / methanol / 3 h / 50 °C

3: methanol

4: 1.) dicyclohexylcarbodiimide (DCC) / 1.) pyridine, room temp.; 2.) H₂O

With hydrogenchloride; ammonia; dicyclohexyl-carbodiimide; In methanol;
DOI:10.1248/cpb.33.1458