diphenyl-μ-disulfido-1,2-dithio-dicarbonimidic acid dimethyl ester

Base Information

• Chemical Name: diphenyl-μ-disulfido-1,2-dithio-dicarbonimidic acid dimethyl ester
• CAS No.: 219500-78-4
• Molecular Formula: C₁₆H₁₆N₂S₄
• Molecular Weight: 364.58
• Mol file: 219500-78-4.mol

Synonyms:diphenyl-μ-disulfido-1,2-dithio-dicarbonimidic acid dimethyl ester

Chemical Property of diphenyl-μ-disulfido-1,2-dithio-dicarbonimidic acid dimethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diphenyl-μ-disulfido-1,2-dithio-dicarbonimidic acid dimethyl ester

There total 5 articles about diphenyl-μ-disulfido-1,2-dithio-dicarbonimidic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl N-phenyldithiocarbamate (701-73-5) → diphenyl-μ-disulfido-1,2-dithio-dicarbonimidic acid dimethyl ester (219500-78-4)

Guidance literature:

Multi-step reaction with 2 steps

1: MCPBA, NaHCO₃ / CH₂Cl₂ / 4 h / 0 °C

2: 1 h / 20 °C

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;

DOI:10.1016/S0040-4039(98)02033-4

Reference yield:

C8H9NOS2 → diphenyl-μ-disulfido-1,2-dithio-dicarbonimidic acid dimethyl ester (219500-78-4)

Guidance literature:

at 20 ℃; for 1h; Yield given;

DOI:10.1016/S0040-4039(98)02033-4

Reference yield:

methyl N-phenyldithiocarbamate (701-73-5) → diphenyl-μ-disulfido-1,2-dithio-dicarbonimidic acid dimethyl ester (219500-78-4)

Guidance literature:

With ethanol; iron(III) chloride;

upstream raw materials:

methyl N-phenyldithiocarbamate

sodium ethanolate

ethanol

iodine

Downstream raw materials:

Dimethyldisulphide

phenyl isothiocyanate

methyl N-phenyldithiocarbamate