2-(4-Nitrophenoxy)naphthalene

Base Information

• Chemical Name: 2-(4-Nitrophenoxy)naphthalene
• CAS No.: 71311-82-5
• Molecular Formula: C16H11 N O3
• Molecular Weight: 265.268
• Hs Code.: 2909309090
• DSSTox Substance ID: DTXSID60354031
• Nikkaji Number: J32.585F
• Wikidata: Q82131953
• Mol file: 71311-82-5.mol

Synonyms:2-(4-nitrophenoxy)naphthalene;71311-82-5;Naphthalene, 2-(4-nitrophenoxy)-;Oprea1_174888;SCHEMBL1283188;DTXSID60354031;ORYXOTYJSALBQZ-UHFFFAOYSA-N;WCA31182;MFCD00427410;STK268945;AKOS003244946;4-(naphthalen-2-yloxy)-1-nitrobenzene;CS-0455145;N0807;8N-034;T72865;SR-01000390967;SR-01000390967-1

Chemical Property of 2-(4-Nitrophenoxy)naphthalene

Chemical Property:

• Vapor Pressure: 7.71E-07mmHg at 25°C
• Refractive Index: 1.671
• Boiling Point: 418.9°C at 760 mmHg
• Flash Point: 183.6°C
• PSA: 55.05000
• Density: 1.287g/cm³
• LogP: 5.06350
• Solubility.: soluble in Acetone
• XLogP3: 4.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 265.07389321
• Heavy Atom Count: 20
• Complexity: 333

Purity/Quality:

98%,99%, ^*data from raw suppliers

2-(4-Nitrophenoxy)naphthalene >98.0%(GC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C=C(C=CC2=C1)OC3=CC=C(C=C3)[N+](=O)[O-]

Technology Process of 2-(4-Nitrophenoxy)naphthalene

There total 7 articles about 2-(4-Nitrophenoxy)naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

para-nitrophenyl bromide (586-78-7) + β-naphthol (135-19-3) → 4-nitrophenyl 2-naphthyl ether (71311-82-5)

Guidance literature:

With caesium carbonate; copper(I) bromide; 1,1'-azobis(1-cyanocyclohexanenitrile); In N,N-dimethyl-formamide; at 100 ℃; for 0.5h; Microwave irradiation; Green chemistry;

DOI:10.1016/j.tetlet.2015.02.073

Reference yield: 100.0%

4-Fluoronitrobenzene (350-46-9,178603-76-4) + β-naphthol (135-19-3) → 4-nitrophenyl 2-naphthyl ether (71311-82-5)

Guidance literature:

With cesium fluoride/clinoptilolite; In dimethyl sulfoxide; at 110 ℃; for 0.15h;

DOI:10.1139/cjc-2015-0300

Reference yield: 97.0%

4-chlorobenzonitrile (100-00-5) + β-naphthol (135-19-3) → 4-nitrophenyl 2-naphthyl ether (71311-82-5)

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide; at 100 ℃; for 1.5h;

DOI:10.1007/s10562-018-2627-6

upstream raw materials:

para-nitrophenyl bromide

β-naphthol

p-nitrobenzene iodide

4-chlorobenzonitrile

Downstream raw materials:

4-(naphthalen-2-yloxy)phenylamine

N-(4-(N-(4-(naphthalen-2-yloxy)phenyl)sulfamoyl)phenyl)acetamide

3,5-dichloro-2-hydroxy-N-(4-(naphthalen-2-yloxy)phenyl)benzamide