Technology Process of methyl 5-(2'-methoxy-4'-methylphenyl)hexanoate
There total 20 articles about methyl 5-(2'-methoxy-4'-methylphenyl)hexanoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
10% palladium on carbon; hydrogen; acetic acid;
In
ethyl acetate;
for 24h;
under 1520.1 Torr;
DOI:10.1080/00397910903174382
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridine / Ambient temperature
2: 63 percent / NaBH4 / dimethylsulfoxide / 3 h / 80 °C
3: 89 percent / triphenylphosphine, imidazole, iodine / acetonitrile; diethyl ether / 0.5 h / 0 °C
4: 98 percent / dimethylformamide / Ambient temperature
5: 2N NaOH / ethanol / 12 h / Heating
With
1H-imidazole; sodium hydroxide; sodium tetrahydroborate; iodine; triphenylphosphine;
In
pyridine; diethyl ether; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1248/cpb.43.553
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 63 percent / NaBH4 / dimethylsulfoxide / 3 h / 80 °C
2: 89 percent / triphenylphosphine, imidazole, iodine / acetonitrile; diethyl ether / 0.5 h / 0 °C
3: 98 percent / dimethylformamide / Ambient temperature
4: 2N NaOH / ethanol / 12 h / Heating
With
1H-imidazole; sodium hydroxide; sodium tetrahydroborate; iodine; triphenylphosphine;
In
diethyl ether; ethanol; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1248/cpb.43.553
