N-[3-(2,6-dibromo-4-iodophenoxy)propyl]-N-methyl-2-nitrobenzenesulfonamide

Base Information

Chemical Name:N-[3-(2,6-dibromo-4-iodophenoxy)propyl]-N-methyl-2-nitrobenzenesulfonamide
CAS No.:865722-90-3
Molecular Formula:C₁₆H₁₅Br₂IN₂O₅S
Molecular Weight:634.084
Hs Code.:

Synonyms:N-[3-(2,6-dibromo-4-iodophenoxy)propyl]-N-methyl-2-nitrobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[3-(2,6-dibromo-4-iodophenoxy)propyl]-N-methyl-2-nitrobenzenesulfonamide

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Technology Process of N-[3-(2,6-dibromo-4-iodophenoxy)propyl]-N-methyl-2-nitrobenzenesulfonamide

There total 5 articles about N-[3-(2,6-dibromo-4-iodophenoxy)propyl]-N-methyl-2-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 865722-89-0
N-[3-(2,6-dibromo-4-iodophenoxy)propyl]-2-nitrobenzenesulfonamide

: 67-56-1
methanol

: 865722-90-3
N-[3-(2,6-dibromo-4-iodophenoxy)propyl]-N-methyl-2-nitrobenzenesulfonamide

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In toluene; at 20 ℃; for 0.333333h;
DOI:10.1021/ol0513286

Reference yield:

: 865722-99-2
N-(3-bromopropyl)-2-nitrobenzenesulfonamide

: 865722-90-3
N-[3-(2,6-dibromo-4-iodophenoxy)propyl]-N-methyl-2-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Cs₂CO₃; NaI / acetonitrile / 6 h / 50 °C

2: 94 percent / PPh₃; DEAD / toluene / 0.33 h / 20 °C

With caesium carbonate; triphenylphosphine; sodium iodide; diethylazodicarboxylate; In toluene; acetonitrile;
DOI:10.1021/ol0513286

Reference yield:

: 540-38-5
p-Iodophenol

: 865722-90-3
N-[3-(2,6-dibromo-4-iodophenoxy)propyl]-N-methyl-2-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / N-bromo-tert-butylamine / various solvent(s) / 0.75 h / 0 °C

2: 70 percent / Cs₂CO₃; NaI / acetonitrile / 6 h / 50 °C

3: 94 percent / PPh₃; DEAD / toluene / 0.33 h / 20 °C

With N-bromo-2-methylpropan-2-amine; caesium carbonate; triphenylphosphine; sodium iodide; diethylazodicarboxylate; In toluene; acetonitrile;
DOI:10.1021/ol0513286