Methyl-2-methyl-3-p-fluorphenylpropionat

Base Information

Chemical Name:Methyl-2-methyl-3-p-fluorphenylpropionat
CAS No.:29417-80-9
Molecular Formula:C₁₁H₁₃FO₂
Molecular Weight:196.221
Hs Code.:

Synonyms:Methyl-2-methyl-3-p-fluorphenylpropionat

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl-2-methyl-3-p-fluorphenylpropionat

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Technology Process of Methyl-2-methyl-3-p-fluorphenylpropionat

There total 2 articles about Methyl-2-methyl-3-p-fluorphenylpropionat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 554-12-1
propanoic acid methyl ester

: 459-46-1
4-Fluorobenzyl bromide

: 29417-80-9
Methyl-2-methyl-3-p-fluorphenylpropionat

Guidance literature:: propanoic acid methyl ester; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

4-Fluorobenzyl bromide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 12h;
DOI:10.1002/anie.202108534

Reference yield:

: 554-12-1
propanoic acid methyl ester

: 352-11-4
1-chloromethyl-4-fluorobenzene

: 29417-80-9
Methyl-2-methyl-3-p-fluorphenylpropionat

Guidance literature:: propanoic acid methyl ester; With sodium hydride; In tetrahydrofuran; at 40 - 50 ℃; for 2h;

1-chloromethyl-4-fluorobenzene; In tetrahydrofuran; at 55 - 60 ℃; for 3h;

Reference yield: 66.0%

: 75-77-4
chloro-trimethyl-silane

: 29417-80-9
Methyl-2-methyl-3-p-fluorphenylpropionat

: C₁₄H₂₁FO₂Si

Guidance literature:: With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2h; diastereoselective reaction;
DOI:10.1002/anie.202108534