1-N-methyl-piperazinomethyl-3-[1-(4-isobutylphenyl)ethyl]-4-[3-(p-anisyl)-4-sydnonylidene]amino-1,2,4-triazol-5-thione

Base Information

Chemical Name:1-N-methyl-piperazinomethyl-3-[1-(4-isobutylphenyl)ethyl]-4-[3-(p-anisyl)-4-sydnonylidene]amino-1,2,4-triazol-5-thione
CAS No.:1394249-07-0
Molecular Formula:C₃₀H₃₈N₈O₃S
Molecular Weight:590.75
Hs Code.:

Synonyms:1-N-methyl-piperazinomethyl-3-[1-(4-isobutylphenyl)ethyl]-4-[3-(p-anisyl)-4-sydnonylidene]amino-1,2,4-triazol-5-thione

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Chemical Property of 1-N-methyl-piperazinomethyl-3-[1-(4-isobutylphenyl)ethyl]-4-[3-(p-anisyl)-4-sydnonylidene]amino-1,2,4-triazol-5-thione

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Technology Process of 1-N-methyl-piperazinomethyl-3-[1-(4-isobutylphenyl)ethyl]-4-[3-(p-anisyl)-4-sydnonylidene]amino-1,2,4-triazol-5-thione

There total 7 articles about 1-N-methyl-piperazinomethyl-3-[1-(4-isobutylphenyl)ethyl]-4-[3-(p-anisyl)-4-sydnonylidene]amino-1,2,4-triazol-5-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 109-01-3
1-methyl-piperazine

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1394248-95-3
3-[1-(4-isobutylphenyl)ethyl]-4-[3-(p-anisyl)-4-sydnonylidene]amino-5-mercapto-1,2,4-triazole

: 1394249-07-0
1-N-methyl-piperazinomethyl-3-[1-(4-isobutylphenyl)ethyl]-4-[3-(p-anisyl)-4-sydnonylidene]amino-1,2,4-triazol-5-thione

Guidance literature:: In ethanol; N,N-dimethyl-formamide; at 20 ℃; for 4.5h; regioselective reaction;
DOI:10.1016/j.ejmech.2012.06.011

Reference yield:

: 52827-01-7
2-((4-methoxyphenyl)(nitroso)amino)acetic acid

: 1394249-07-0
1-N-methyl-piperazinomethyl-3-[1-(4-isobutylphenyl)ethyl]-4-[3-(p-anisyl)-4-sydnonylidene]amino-1,2,4-triazol-5-thione

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic anhydride / Heating

2.1: trichlorophosphate / 0.5 h

2.2: 45 °C

3.1: sulfuric acid / ethanol / 20 °C

4.1: ethanol; N,N-dimethyl-formamide / 4.5 h / 20 °C

With sulfuric acid; acetic anhydride; trichlorophosphate; In ethanol; N,N-dimethyl-formamide; 4.1: Mannich reaction;
DOI:10.1016/j.ejmech.2012.06.011

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1394249-07-0
1-N-methyl-piperazinomethyl-3-[1-(4-isobutylphenyl)ethyl]-4-[3-(p-anisyl)-4-sydnonylidene]amino-1,2,4-triazol-5-thione

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium acetate / ethanol / 6 h / Reflux

2.1: sodium hydroxide / water / 0.5 h / Reflux

2.2: pH 2

3.1: hydrogenchloride; sodium nitrite / water / 2.5 h / 0 °C

4.1: acetic anhydride / Heating

5.1: trichlorophosphate / 0.5 h

5.2: 45 °C

6.1: sulfuric acid / ethanol / 20 °C

7.1: ethanol; N,N-dimethyl-formamide / 4.5 h / 20 °C

With hydrogenchloride; sulfuric acid; sodium acetate; acetic anhydride; sodium hydroxide; sodium nitrite; trichlorophosphate; In ethanol; water; N,N-dimethyl-formamide; 7.1: Mannich reaction;
DOI:10.1016/j.ejmech.2012.06.011