ethyl 3-(4-ethylphenyl)-2-propynoate

Base Information

Chemical Name:ethyl 3-(4-ethylphenyl)-2-propynoate
CAS No.:887274-55-7
Molecular Formula:C₁₃H₁₄O₂
Molecular Weight:202.253
Hs Code.:

Synonyms:ethyl 3-(4-ethylphenyl)-2-propynoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 3-(4-ethylphenyl)-2-propynoate

Chemical Property:

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Technology Process of ethyl 3-(4-ethylphenyl)-2-propynoate

There total 3 articles about ethyl 3-(4-ethylphenyl)-2-propynoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63139-21-9
4-ethylphenylboronic acid

: 623-47-2
propynoic acid ethyl ester

: 887274-55-7
ethyl 3-(4-ethylphenyl)-2-propynoate

Guidance literature:: With copper(l) iodide; caesium carbonate; silver(l) oxide; In 1,2-dichloro-ethane; at 80 ℃; for 36h;
DOI:10.1039/c3cc48308h

Reference yield:

: 25309-64-2
4-ethyl-1-iodobenzene

: 623-47-2
propynoic acid ethyl ester

: 887274-55-7
ethyl 3-(4-ethylphenyl)-2-propynoate

Guidance literature:: With copper(l) iodide; potassium carbonate; In tetrahydrofuran; at 65 ℃; for 24h; Inert atmosphere;
DOI:10.1002/anie.201611214

Reference yield:

: 74-96-4
ethyl bromide

: 124-38-9,18923-20-1
carbon dioxide

: 40307-11-7
1-ethyl-4-ethynylbenzene

: 887274-55-7
ethyl 3-(4-ethylphenyl)-2-propynoate

Guidance literature:: With caesium carbonate; triphenylphosphine; copper(l) chloride; In N,N-dimethyl-formamide; at 80 ℃; for 4h; Sealed tube; Green chemistry;
DOI:10.1039/c5gc00926j