N'1.N'2-bis(2-chloropropanoyl)-4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)phthalohydrazide

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Chemical Name:N'1.N'2-bis(2-chloropropanoyl)-4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)phthalohydrazide
CAS No.:1309588-15-5
Molecular Formula:C₂₈H₃₃Cl₂N₇O₄S
Molecular Weight:634.587
Hs Code.:

Synonyms:N'1.N'2-bis(2-chloropropanoyl)-4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)phthalohydrazide

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Chemical Property of N'1.N'2-bis(2-chloropropanoyl)-4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)phthalohydrazide

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Technology Process of N'1.N'2-bis(2-chloropropanoyl)-4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)phthalohydrazide

There total 5 articles about N'1.N'2-bis(2-chloropropanoyl)-4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)phthalohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1309588-09-7
4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)phthalohydrazide

: 625-36-5
2-chloropropionyl chloride

: 1309588-15-5
N'1.N'2-bis(2-chloropropanoyl)-4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)phthalohydrazide

Guidance literature:: With triethylamine; In benzene; for 10h; Reflux;
DOI:10.1007/s00044-010-9389-z

Reference yield:

: 1309588-06-4
4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)phthalic acid

: 1309588-15-5
N'1.N'2-bis(2-chloropropanoyl)-4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)phthalohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / 4 h / Reflux

1.2: 6 h / Reflux

2.1: triethylamine / benzene / 10 h / Reflux

With thionyl chloride; triethylamine; In benzene;
DOI:10.1007/s00044-010-9389-z

Reference yield:

: 306963-81-5
2-(2-(4-isobutylphenyl)propanoyl)hydrazinecarbothioamide

: 1309588-15-5
N'1.N'2-bis(2-chloropropanoyl)-4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)phthalohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; potassium hydroxide / water / Reflux

2.1: ethanol / 4 h / Reflux

3.1: thionyl chloride / 4 h / Reflux

3.2: 6 h / Reflux

4.1: triethylamine / benzene / 10 h / Reflux

With hydrogenchloride; thionyl chloride; triethylamine; potassium hydroxide; In ethanol; water; benzene;
DOI:10.1007/s00044-010-9389-z