methyl 3-(tert-butoxycarbonyl(isopropyl)amino)-2-(4-chlorophenyl)propanoate

Base Information

Chemical Name:methyl 3-(tert-butoxycarbonyl(isopropyl)amino)-2-(4-chlorophenyl)propanoate
CAS No.:1000985-04-5
Molecular Formula:C₁₈H₂₆ClNO₄
Molecular Weight:355.862
Hs Code.:

Synonyms:methyl 3-(tert-butoxycarbonyl(isopropyl)amino)-2-(4-chlorophenyl)propanoate

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Chemical Property of methyl 3-(tert-butoxycarbonyl(isopropyl)amino)-2-(4-chlorophenyl)propanoate

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Technology Process of methyl 3-(tert-butoxycarbonyl(isopropyl)amino)-2-(4-chlorophenyl)propanoate

There total 6 articles about methyl 3-(tert-butoxycarbonyl(isopropyl)amino)-2-(4-chlorophenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 50415-59-3
methyl 2-(4-chlorophenyl)acrylate

: 75-31-0
isopropylamine

: 1000985-04-5
methyl 3-(tert-butoxycarbonyl(isopropyl)amino)-2-(4-chlorophenyl)propanoate

Guidance literature:: methyl 2-(4-chlorophenyl)acrylate; isopropylamine; In tetrahydrofuran; at 0 - 20 ℃;

di-tert-butyl dicarbonate; In tetrahydrofuran;

Reference yield:

: 1000985-03-4
methyl 2-(4-chlorophenyl)-3-(isopropylamino)propanoate

: 24424-99-5
di-tert-butyl dicarbonate

: 1000985-04-5
methyl 3-(tert-butoxycarbonyl(isopropyl)amino)-2-(4-chlorophenyl)propanoate

Guidance literature:: dmap; In dichloromethane; at 20 ℃;

Reference yield:

: 1878-66-6
4-chlorophenylacetic Acid

: 1000985-04-5
methyl 3-(tert-butoxycarbonyl(isopropyl)amino)-2-(4-chlorophenyl)propanoate

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid / 20 °C

2: sodium methylate / dimethyl sulfoxide / 2 h / 20 °C

3: methanesulfonyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C

4: tetrahydrofuran / 0 - 20 °C

5: tetrahydrofuran

With sulfuric acid; sodium methylate; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide;