N-(2-bromo-4-(1-methylethyl)phenyl)-N-ethyl-4,6-dimethyl-2-pyrimidinamine

Base Information

Chemical Name:N-(2-bromo-4-(1-methylethyl)phenyl)-N-ethyl-4,6-dimethyl-2-pyrimidinamine
CAS No.:169882-41-1
Molecular Formula:C₁₇H₂₂BrN₃
Molecular Weight:348.286
Hs Code.:

Synonyms:N-(2-bromo-4-(1-methylethyl)phenyl)-N-ethyl-4,6-dimethyl-2-pyrimidinamine

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Chemical Property of N-(2-bromo-4-(1-methylethyl)phenyl)-N-ethyl-4,6-dimethyl-2-pyrimidinamine

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Technology Process of N-(2-bromo-4-(1-methylethyl)phenyl)-N-ethyl-4,6-dimethyl-2-pyrimidinamine

There total 6 articles about N-(2-bromo-4-(1-methylethyl)phenyl)-N-ethyl-4,6-dimethyl-2-pyrimidinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 75-03-6
ethyl iodide

: 169882-90-0
2-N-(2-bromo-4-(1-methylethyl)phenyl)-4,6-dimethyl-2-pyrimidinamine

: 169882-41-1
N-(2-bromo-4-(1-methylethyl)phenyl)-N-ethyl-4,6-dimethyl-2-pyrimidinamine

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 16h; Ambient temperature;
DOI:10.1021/jm980222w

Reference yield:

: 51605-97-1
2-bromo-4-isopropylaniline

: 169882-41-1
N-(2-bromo-4-(1-methylethyl)phenyl)-N-ethyl-4,6-dimethyl-2-pyrimidinamine

Guidance literature:: Multi-step reaction with 3 steps

1: HCl / 1.) AcOEt, EtOH, ether, RT, 1 h, 2.) AOEt, EtOH, reflux, 3 h

2: K₂CO₃ / dimethylformamide / 24 h / Heating

3: 73 percent / NaH / tetrahydrofuran / 16 h / Ambient temperature

With hydrogenchloride; sodium hydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm980222w

Reference yield:

: 2-bromo-4-(1-methylethyl)phenylguanidinium hydrochloride

: 169882-41-1
N-(2-bromo-4-(1-methylethyl)phenyl)-N-ethyl-4,6-dimethyl-2-pyrimidinamine

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide / 24 h / Heating

2: 73 percent / NaH / tetrahydrofuran / 16 h / Ambient temperature

With sodium hydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm980222w