O-ethyl S-triphenylmethyl dithiocarbonate

Base Information

• Chemical Name: O-ethyl S-triphenylmethyl dithiocarbonate
• CAS No.: 132277-76-0
• Molecular Formula: C₂₂H₂₀OS₂
• Molecular Weight: 364.532
• Mol file: 132277-76-0.mol

Synonyms:O-ethyl S-triphenylmethyl dithiocarbonate

Chemical Property of O-ethyl S-triphenylmethyl dithiocarbonate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of O-ethyl S-triphenylmethyl dithiocarbonate

There total 4 articles about O-ethyl S-triphenylmethyl dithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

bromo-triphenyl-methane (596-43-0) + potassium ethyl xanthogenate (140-89-6) → benzophenone (119-61-9) + triphenylmethyl alcohol (76-84-6) + bis-ethoxythiocarbonyldisulfane (502-55-6) + ditrityl peroxide (596-30-5) + O-ethyl S-triphenylmethyl dithiocarbonate (132277-76-0)

Guidance literature:

With oxygen; In benzene; for 52h; Product distribution; Mechanism; Ambient temperature; variation of time;

DOI:10.1039/P29900002009

Reference yield: 2.0%

bromo-triphenyl-methane (596-43-0) + potassium ethyl xanthogenate (140-89-6) → triphenylmethyl alcohol (76-84-6) + bis-ethoxythiocarbonyldisulfane (502-55-6) + O-ethyl S-triphenylmethyl dithiocarbonate (132277-76-0)

Guidance literature:

In benzene; for 6h; Ambient temperature;

DOI:10.1039/P29900002009

Reference yield: 1.0%

bromo-triphenyl-methane (596-43-0) + potassium ethyl xanthogenate (140-89-6) → benzophenone (119-61-9) + triphenylmethyl alcohol (76-84-6) + bis-ethoxythiocarbonyldisulfane (502-55-6) + triphenylmethane (519-73-3) + O-ethyl S-triphenylmethyl dithiocarbonate (132277-76-0)

Guidance literature:

In various solvent(s); at 100 ℃; for 9h; Product distribution; Mechanism; variation of solvent, time ,temperature;

DOI:10.1039/P29900002009

upstream raw materials:

O-ethyl hydrogen dithiocarbonate

trityl chloride

bromo-triphenyl-methane

potassium ethyl xanthogenate

Refernces