(α-Benzoylbenzyl)diphenylphosphanoxid

Base Information

Chemical Name:(α-Benzoylbenzyl)diphenylphosphanoxid
CAS No.:76202-75-0
Molecular Formula:C₂₆H₂₁O₂P
Molecular Weight:396.425
Hs Code.:

Synonyms:(α-Benzoylbenzyl)diphenylphosphanoxid

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Chemical Property of (α-Benzoylbenzyl)diphenylphosphanoxid

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Technology Process of (α-Benzoylbenzyl)diphenylphosphanoxid

There total 7 articles about (α-Benzoylbenzyl)diphenylphosphanoxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 19690-01-8
1,2-diphenylethanone O-acetyl oxime

: 4559-70-0
Diphenylphosphine oxide

: 76202-75-0
(α-Benzoylbenzyl)diphenylphosphanoxid

Guidance literature:: 1,2-diphenylethanone O-acetyl oxime; Diphenylphosphine oxide; With acetic anhydride; copper(l) chloride; tricyclohexylphosphine; In 1,4-dioxane; at 130 ℃; Inert atmosphere;

With hydrogenchloride; In water; at 60 - 100 ℃;
DOI:10.1039/d0cc07770d

Reference yield:

: 952-06-7
deoxybenzoin oxime

: 76202-75-0
(α-Benzoylbenzyl)diphenylphosphanoxid

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; pyridine / 1 h / 20 °C / Sealed tube

2: copper(l) chloride; tricyclohexylphosphine / 1,4-dioxane / 5 h / 130 °C / Sealed tube; Inert atmosphere

3: hydrogenchloride; water / 0.5 h / 20 °C / Sealed tube

With pyridine; hydrogenchloride; dmap; water; copper(l) chloride; tricyclohexylphosphine; In 1,4-dioxane;
DOI:10.1002/anie.201501287

Reference yield:

: 451-40-1
phenyl benzyl ketone

: 76202-75-0
(α-Benzoylbenzyl)diphenylphosphanoxid

Guidance literature:: Multi-step reaction with 4 steps

1: hydroxylamine hydrochloride; pyridine / ethanol / 1 h / 60 °C / Sealed tube

2: dmap; pyridine / 1 h / 20 °C / Sealed tube

3: copper(l) chloride; tricyclohexylphosphine / 1,4-dioxane / 5 h / 130 °C / Sealed tube; Inert atmosphere

4: hydrogenchloride; water / 0.5 h / 20 °C / Sealed tube

With pyridine; hydrogenchloride; dmap; hydroxylamine hydrochloride; water; copper(l) chloride; tricyclohexylphosphine; In 1,4-dioxane; ethanol;
DOI:10.1002/anie.201501287