C₃₉H₄₉NO₃S₂Si

Base Information

Chemical Name:C₃₉H₄₉NO₃S₂Si
CAS No.:1410797-75-9
Molecular Formula:C₃₉H₄₉NO₃S₂Si
Molecular Weight:672.04
Hs Code.:

C<sub>39</sub>H<sub>49</sub>NO<sub>3</sub>S<sub>2</sub>Si

Synonyms:C₃₉H₄₉NO₃S₂Si

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Chemical Property of C₃₉H₄₉NO₃S₂Si

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Technology Process of C₃₉H₄₉NO₃S₂Si

There total 9 articles about C₃₉H₄₉NO₃S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₄H₄₇NO₆S₂Si

: 930-69-8
sodium thiophenolate

: 1410797-75-9
C₃₉H₄₉NO₃S₂Si

: C₃₂H₄₁NO₃SSi

Guidance literature:: In tetrahydrofuran; for 24h; Reflux;
DOI:10.1016/j.tet.2012.08.043

Reference yield:

: 127793-62-8
4-((tert-butyldiphenylsilyl)oxy)butanal

: 1410797-75-9
C₃₉H₄₉NO₃S₂Si

: C₃₂H₄₁NO₃SSi

Guidance literature:: Multi-step reaction with 9 steps

1.1: tetrahydrofuran / -40 °C / Inert atmosphere

2.1: propionic acid / 4 h / 138 °C

3.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 - 20 °C

4.1: triethylamine / tetrahydrofuran / 1.5 h / 0 - 20 °C

5.1: potassium hydroxide / N,N-dimethyl-formamide / 0.5 h / 120 °C

5.2: 5 h / 120 °C

6.1: oxone; tetra(n-butyl)ammonium hydrogensulfate; disodium ethylenediaminetetraacetic acid; potassium carbonate; acetic acid / acetonitrile / 0 °C

7.1: (1S)-10-camphorsulfonic acid / dichloromethane / 1.5 h / 25 °C

8.1: triethylamine / tetrahydrofuran / 3 h / 0 - 25 °C

9.1: tetrahydrofuran / 24 h / Reflux

With lithium aluminium tetrahydride; oxone; (1S)-10-camphorsulfonic acid; tetra(n-butyl)ammonium hydrogensulfate; disodium ethylenediaminetetraacetic acid; potassium carbonate; acetic acid; propionic acid; triethylamine; potassium hydroxide; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile; 2.1: |Johnson-Claisen Rearrangement;
DOI:10.1016/j.tet.2012.08.043

Reference yield:

: C₂₅H₃₆O₄SSi

: 1410797-75-9
C₃₉H₄₉NO₃S₂Si

: C₃₂H₄₁NO₃SSi

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / N,N-dimethyl-formamide / 0.5 h / 120 °C

1.2: 5 h / 120 °C

2.1: oxone; tetra(n-butyl)ammonium hydrogensulfate; disodium ethylenediaminetetraacetic acid; potassium carbonate; acetic acid / acetonitrile / 0 °C

3.1: (1S)-10-camphorsulfonic acid / dichloromethane / 1.5 h / 25 °C

4.1: triethylamine / tetrahydrofuran / 3 h / 0 - 25 °C

5.1: tetrahydrofuran / 24 h / Reflux

With oxone; (1S)-10-camphorsulfonic acid; tetra(n-butyl)ammonium hydrogensulfate; disodium ethylenediaminetetraacetic acid; potassium carbonate; acetic acid; triethylamine; potassium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2012.08.043