N-cyclohexyl-1,2-benzothiazol-3-amine 1,1-dioxide

Base Information

Chemical Name:N-cyclohexyl-1,2-benzothiazol-3-amine 1,1-dioxide
CAS No.:7668-22-6
Molecular Formula:C₁₃H₁₆N₂O₂S
Molecular Weight:264.348
Hs Code.:

Synonyms:1,2-Benzisothiazole,3-(cyclohexylamino)-, 1,1-dioxide (6CI,7CI,8CI);N-(1,1-Dioxobenzo[d]isothiazol-3-yl)cyclohexylamine; NSC 331992

Suppliers and Price of N-cyclohexyl-1,2-benzothiazol-3-amine 1,1-dioxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of N-cyclohexyl-1,2-benzothiazol-3-amine 1,1-dioxide

Chemical Property:

Vapor Pressure:5.2E-08mmHg at 25°C
Boiling Point:442°C at 760 mmHg
Flash Point:221.1°C
Density:1.42g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-cyclohexyl-1,2-benzothiazol-3-amine 1,1-dioxide

There total 4 articles about N-cyclohexyl-1,2-benzothiazol-3-amine 1,1-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 4998-76-9
cyclohexylamine hydrochloride

: 81-07-2
saccharin

: 7668-22-6
N-(1,1-dioxobenzo[d]isothiazol-3-yl)cyclohexylamine

Guidance literature:: With N,N-dimethyl-cyclohexanamine; phosphorus pentoxide; at 240 ℃; for 2h;

Reference yield: 25.0%

: 108-91-8,157973-60-9
cyclohexylamine

: 567-19-1
3-chloro-1,2-benzisothiazole 1,1-dioxide

: 7668-22-6
N-(1,1-dioxobenzo[d]isothiazol-3-yl)cyclohexylamine

Guidance literature:: In chloroform; at 20 ℃; Inert atmosphere;
DOI:10.1021/acsmedchemlett.7b00137

Reference yield:

: 81-07-2
saccharin

: 7668-22-6
N-(1,1-dioxobenzo[d]isothiazol-3-yl)cyclohexylamine

Guidance literature:: Multi-step reaction with 2 steps

1: dichlorotriphenyl-λ⁴-phosphane; triethylamine / chloroform / 0 - 35 °C / Inert atmosphere

2: chloroform / 20 °C / Inert atmosphere

With dichlorotriphenyl-λ⁴-phosphane; triethylamine; In chloroform;
DOI:10.1021/acsmedchemlett.7b00137