2-fluoro-1,4-dichloromethylbenzene

Base Information

Chemical Name:2-fluoro-1,4-dichloromethylbenzene
CAS No.:127865-67-2
Molecular Formula:C₈H₇Cl₂F
Molecular Weight:193.048
Hs Code.:

Synonyms:2-fluoro-1,4-dichloromethylbenzene

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Chemical Property of 2-fluoro-1,4-dichloromethylbenzene

Chemical Property:

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Technology Process of 2-fluoro-1,4-dichloromethylbenzene

There total 3 articles about 2-fluoro-1,4-dichloromethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 696-01-5
2-fluoro-1,4-dimethylbenzene

: 147542-00-5
4-(chloromethyl)-2-fluoro-1-methylbenzene

: 147541-99-9
2-fluoro-4-methylbenzyl chloride

: 127865-67-2
2-fluoro-1,4-dichloromethylbenzene

Guidance literature:: With sulfuryl dichloride; 2,2'-azobis(isobutyronitrile); at 100 ℃; for 9h;
DOI:10.1016/S0022-1139(00)82933-4

Reference yield:

: 89-58-7
mononitro-p-xylene

: 127865-67-2
2-fluoro-1,4-dichloromethylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / 85percent hydrazine hydrate / Raney-Ni / ethanol / 1 h / 90 °C

2: 1) NaNO2, HCl, NaBF4 / 1) water, 25 deg C, 1h, 2) Δ

3: 46 percent / SO₂Cl₂ / azobisisobutyronitrile / 9 h / 100 °C

With hydrogenchloride; sodium tetrafluoroborate; sulfuryl dichloride; hydrazine hydrate; sodium nitrite; 2,2'-azobis(isobutyronitrile); nickel; In ethanol;
DOI:10.1016/S0022-1139(00)82933-4

Reference yield:

: 95-78-3
2,5-Dimethylaniline

: 127865-67-2
2-fluoro-1,4-dichloromethylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaNO2, HCl, NaBF4 / 1) water, 25 deg C, 1h, 2) Δ

2: 46 percent / SO₂Cl₂ / azobisisobutyronitrile / 9 h / 100 °C

With hydrogenchloride; sodium tetrafluoroborate; sulfuryl dichloride; sodium nitrite; 2,2'-azobis(isobutyronitrile);
DOI:10.1016/S0022-1139(00)82933-4