N-2-chloro-5-(3-chloro-5-trifluoromethyl-2-pyridyl)phenylhydroxylamine

Base Information

Chemical Name:N-2-chloro-5-(3-chloro-5-trifluoromethyl-2-pyridyl)phenylhydroxylamine
CAS No.:197446-79-0
Molecular Formula:C₁₂H₇Cl₂F₃N₂O
Molecular Weight:323.102
Hs Code.:

Synonyms:N-2-chloro-5-(3-chloro-5-trifluoromethyl-2-pyridyl)phenylhydroxylamine

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Chemical Property of N-2-chloro-5-(3-chloro-5-trifluoromethyl-2-pyridyl)phenylhydroxylamine

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Technology Process of N-2-chloro-5-(3-chloro-5-trifluoromethyl-2-pyridyl)phenylhydroxylamine

There total 4 articles about N-2-chloro-5-(3-chloro-5-trifluoromethyl-2-pyridyl)phenylhydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 161949-51-5
2-chloro-5-(3-chloro-5-trifluoromethyl-2-pyridyl)nitrobenzene

: 197446-79-0
N-2-chloro-5-(3-chloro-5-trifluoromethyl-2-pyridyl)phenylhydroxylamine

Guidance literature:: With hydrogen; platinum on activated charcoal; In various solvent(s);
DOI:10.2533/000942903777678650

Reference yield:

: 1679-18-1
4-Chlorophenylboronic acid

: 197446-79-0
N-2-chloro-5-(3-chloro-5-trifluoromethyl-2-pyridyl)phenylhydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / Pd(PPh₃)4; Na₂CO₃

2: 95 percent / HNO₃; H₂SO₄

3: 98 percent / H₂ / Pt/C / various solvent(s)

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; hydrogen; nitric acid; sodium carbonate; platinum on activated charcoal; In various solvent(s); 1: Suzuki coupling;
DOI:10.2533/000942903777678650

Reference yield:

: 69045-84-7
2,3-dichloro-5-trifluoromethylpyridine

: 197446-79-0
N-2-chloro-5-(3-chloro-5-trifluoromethyl-2-pyridyl)phenylhydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / Pd(PPh₃)4; Na₂CO₃

2: 95 percent / HNO₃; H₂SO₄

3: 98 percent / H₂ / Pt/C / various solvent(s)

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; hydrogen; nitric acid; sodium carbonate; platinum on activated charcoal; In various solvent(s); 1: Suzuki coupling;
DOI:10.2533/000942903777678650