N-Methoxy-N,2-dimethylbenzamide

Base Information

Chemical Name:N-Methoxy-N,2-dimethylbenzamide
CAS No.:130250-61-2
Molecular Formula:C10H13 N O2
Molecular Weight:179.219
Hs Code.:2924299090
European Community (EC) Number:847-658-2
DSSTox Substance ID:DTXSID00462942
Nikkaji Number:J3.195.313H
Wikidata:Q82287598
Mol file:130250-61-2.mol

Synonyms:N-Methoxy-N,2-dimethylbenzamide;130250-61-2;2,N-DIMETHYL-N-METHOXYBENZAMIDE;n-methoxy-2,n-dimethylbenzamide;SCHEMBL4611372;N-Methoxy-2, N-dimethybenzamide;DTXSID00462942;n-methoxy-2, n-dimethylbenzamide;VXCBISJCEBDQAL-UHFFFAOYSA-N;MFCD02684309;AKOS008952799;FT-0691492;C77847;EN300-1228443;Z54740153;F1903-0113

Suppliers and Price of N-Methoxy-N,2-dimethylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
N-Methoxy-N,2-dimethylbenzamide 95+%
5g
$ 422.00

American Custom Chemicals Corporation
2,N-DIMETHYL-N-METHOXYBENZAMIDE 95.00%
5G
$ 1249.13

Alichem
N-Methoxy-N,2-dimethylbenzamide
5g
$ 344.00

Acrotein
N-Methoxy-N,2-dimethylbenzamide 97%
1g
$ 91.67

Total 16 raw suppliers

Chemical Property of N-Methoxy-N,2-dimethylbenzamide

Chemical Property:

Vapor Pressure:0.000407mmHg at 25°C
Refractive Index:1.523
Boiling Point:316.6°C at 760 mmHg
Flash Point:145.2°C
PSA：29.54000
Density:1.07g/cm³
LogP:1.62840
Storage Temp.:2-8°C
XLogP3:1.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:179.094628657
Heavy Atom Count:13
Complexity:182

Purity/Quality:

98%min ^*data from raw suppliers

N-Methoxy-N,2-dimethylbenzamide 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=CC=C1C(=O)N(C)OC

Technology Process of N-Methoxy-N,2-dimethylbenzamide

There total 11 articles about N-Methoxy-N,2-dimethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 89-71-4
2-Methyl-benzoic acid methyl ester

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 130250-61-2
2-methyl-N-methoxy-N-methylbenzamide

Guidance literature:: 2-Methyl-benzoic acid methyl ester; N,O-dimethylhydroxylamine*hydrochloride; In tetrahydrofuran; at -20 ℃; for 0.0833333h; Inert atmosphere;

With isopropylmagnesium chloride; In tetrahydrofuran; diethyl ether; at -20 ℃; for 0.416667h; Inert atmosphere;
DOI:10.1039/c3ob40578h

Reference yield: 96.0%

: 118-90-1
ortho-methylbenzoic acid

: 1117-97-1
N,0-dimethylhydroxylamine

: 130250-61-2
2-methyl-N-methoxy-N-methylbenzamide

Guidance literature:: ortho-methylbenzoic acid; N,0-dimethylhydroxylamine; In toluene; at 0 ℃; for 0.166667h;

With phosphorus trichloride; In toluene; at 20 - 60 ℃; for 0.5h;
DOI:10.1055/s-0033-1340317

Reference yield: 94.0%

: 615-37-2
ortho-methylphenyl iodide

: 201230-82-2
carbon monoxide

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 130250-61-2
2-methyl-N-methoxy-N-methylbenzamide

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; palladium diacetate; sodium carbonate; In acetonitrile; at 80 ℃; for 8h; under 760.051 Torr; Autoclave; Inert atmosphere;
DOI:10.1039/c4ob00729h