ALPHA-METHYLBENZYL ACETATE)

Base Information

• Chemical Name: ALPHA-METHYLBENZYL ACETATE)
• CAS No.: 50373-55-2
• Molecular Formula: C₁₀H₁₂O₂
• Molecular Weight: 164.204
• Mol file: 50373-55-2.mol

Synonyms:

Chemical Property of ALPHA-METHYLBENZYL ACETATE)

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ALPHA-METHYLBENZYL ACETATE)

There total 153 articles about ALPHA-METHYLBENZYL ACETATE) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

Isopropenyl acetate (108-22-5) + 1-Phenylethanol (98-85-1,13323-81-4) → 1-methyl-3-phenyl-butanal (17913-10-9) + 1-phenylethyl acetate (93-92-5,50373-55-2)

Guidance literature:

Isopropenyl acetate; 1-Phenylethanol; With gallium(III) bromide; In dichloromethane; at 40 ℃; for 2h; Inert atmosphere;

With sodium hydrogencarbonate; In diethyl ether; dichloromethane; water;

DOI:10.1002/anie.200904069

Reference yield: 81.0%

benzylidene 1,1-diacetate (581-55-5) → 1-phenylethyl acetate (93-92-5,50373-55-2) + benzaldehyde (100-52-7)

Guidance literature:

With magnesium; In tetrahydrofuran; at 20 ℃; for 3h; Title compound not separated from byproducts; ultrasound irradiation;

DOI:10.1016/S0040-4020(97)00789-8

Reference yield: 80.0%

ethyl acetate (141-78-6) + acetophenone (98-86-2) → 1-Phenylethanol (98-85-1,13323-81-4) + 1-phenylethyl acetate (93-92-5,50373-55-2)

Guidance literature:

With sodium tetrahydroborate; for 7h; Product distribution; Heating; other aldehydes and ketones;

DOI:10.1080/00397919108021569

upstream raw materials:

Perbenzoic acid

3-phenyl-butan-2-one

ethylbenzene

1-Phenylethanol

Downstream raw materials:

styrene

acetic acid

1-phenylethyl acetoacetate

1-Phenylethanol