2-Chloro-5-methylquinoxaline

Base Information

Chemical Name:2-Chloro-5-methylquinoxaline
CAS No.:61148-17-2
Molecular Formula:C9H7ClN2
Molecular Weight:178.621
Hs Code.:2933990090
DSSTox Substance ID:DTXSID80506873
Wikidata:Q82362836
Mol file:61148-17-2.mol

Synonyms:2-Chloro-5-methylquinoxaline;61148-17-2;Quinoxaline, 2-chloro-5-methyl- (9CI);SCHEMBL11842508;DTXSID80506873;GYSCSMIVGRTCQY-UHFFFAOYSA-N;A918455

Suppliers and Price of 2-Chloro-5-methylquinoxaline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-Chloro-5-methylquinoxaline 95+%
1g
$ 510.00

Chemenu
2-chloro-5-methylquinoxaline 95%
1g
$ 482.00

American Custom Chemicals Corporation
2-CHLORO-5-METHYLQUINOXALINE 95.00%
5MG
$ 503.40

Alichem
2-Chloro-5-methylquinoxaline
1g
$ 445.12

Total 7 raw suppliers

Chemical Property of 2-Chloro-5-methylquinoxaline

Chemical Property:

PSA：25.78000
LogP:2.59160
Storage Temp.:2-8°C
XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:178.0297759
Heavy Atom Count:12
Complexity:163

Purity/Quality:

97% ^*data from raw suppliers

2-Chloro-5-methylquinoxaline 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C2C(=CC=C1)N=C(C=N2)Cl

Technology Process of 2-Chloro-5-methylquinoxaline

There total 8 articles about 2-Chloro-5-methylquinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76052-78-3
5-methylquinoxaline-2(1H)-one

: 61148-17-2
2-chloro-5-methylquinoxaline

Guidance literature:: With phosphorus pentachloride; trichlorophosphate;
DOI:10.1021/ja01169a001 DOI:10.1021/ja01177a516

Reference yield:

: 2687-25-4
3-methyl-1,2-benzenediamine

: 61148-17-2
2-chloro-5-methylquinoxaline

Guidance literature:: Multi-step reaction with 2 steps

1: 3 h / Ambient temperature

2: POCl₃ / dimethylformamide / 1.5 h / Heating

With trichlorophosphate; In N,N-dimethyl-formamide;
DOI:10.1021/jm00133a019

Reference yield:

: 924-44-7
glyoxylic acid ethyl ester

: 2687-25-4
3-methyl-1,2-benzenediamine

: 61148-17-2
2-chloro-5-methylquinoxaline

: 61148-40-1
2-chloro-8-methylquinoxaline

Guidance literature:: glyoxylic acid ethyl ester; 3-methyl-1,2-benzenediamine; In ethanol; for 0.5h; Reflux;

With trichlorophosphate; at 110 ℃; for 1h;
DOI:10.1016/j.bmcl.2013.06.048