C₁₅H₂₁IO₂

Base Information

Chemical Name:C₁₅H₂₁IO₂
CAS No.:1627848-04-7
Molecular Formula:C₁₅H₂₁IO₂
Molecular Weight:360.235
Hs Code.:

C<sub>15</sub>H<sub>21</sub>IO<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₁IO₂

Chemical Property:

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Technology Process of C₁₅H₂₁IO₂

There total 6 articles about C₁₅H₂₁IO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: {(2R,3S)-3-[5-(benzyloxy)pentyl]oxiran-2-yl}methanol

: 1627848-04-7
C₁₅H₂₁IO₂

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 1.08333h;
DOI:10.1002/hlca.201300223

Reference yield:

: 629-11-8
1,6-hexanediol

: 1627848-04-7
C₁₅H₂₁IO₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 - 20 °C

1.2: 20 °C

2.1: triethylamine; oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C

3.1: benzene / 0.5 h / Reflux

4.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 0.5 h / -10 - 0 °C

5.1: titanium(IV) isopropylate; diethyl (2S,3S)-tartrate / dichloromethane / 0.5 h / -30 °C / Molecular sieve

5.2: 4 h / -30 °C / Molecular sieve

6.1: 1H-imidazole; triphenylphosphine; iodine / tetrahydrofuran / 1.08 h / 0 - 20 °C

With 1H-imidazole; titanium(IV) isopropylate; oxalyl dichloride; diethyl (2S,3S)-tartrate; iodine; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; toluene; mineral oil; benzene; 2.1: |Swern Oxidation / 3.1: |Wittig Olefination / 5.1: |Sharpless Asymmetric Epoxidation / 5.2: |Sharpless Asymmetric Epoxidation;
DOI:10.1002/hlca.201300223

Reference yield:

: 71126-73-3
6-benzyloxyhexan-1-ol

: 1627848-04-7
C₁₅H₂₁IO₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine; oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C

2.1: benzene / 0.5 h / Reflux

3.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 0.5 h / -10 - 0 °C

4.1: titanium(IV) isopropylate; diethyl (2S,3S)-tartrate / dichloromethane / 0.5 h / -30 °C / Molecular sieve

4.2: 4 h / -30 °C / Molecular sieve

5.1: 1H-imidazole; triphenylphosphine; iodine / tetrahydrofuran / 1.08 h / 0 - 20 °C

With 1H-imidazole; titanium(IV) isopropylate; oxalyl dichloride; diethyl (2S,3S)-tartrate; iodine; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; toluene; benzene; 1.1: |Swern Oxidation / 2.1: |Wittig Olefination / 4.1: |Sharpless Asymmetric Epoxidation / 4.2: |Sharpless Asymmetric Epoxidation;
DOI:10.1002/hlca.201300223