benzyl 2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate

Base Information

Chemical Name:benzyl 2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate
CAS No.:190906-91-3
Molecular Formula:C14H15NO3
Molecular Weight:245.278
Hs Code.:2933399090
DSSTox Substance ID:DTXSID00466581
Nikkaji Number:J1.619.269D
Mol file:190906-91-3.mol

Synonyms:190906-91-3;benzyl 2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate;Benzyl 2-methyl-4-oxo-2,3-dihydropyridine-1-carboxylate;Benzyl 3,4-dihydro-2-methyl-4-oxopyridine-1(2H)-carboxylate;benzyl2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate;SCHEMBL757756;DTXSID00466581;CZZXYDLQRNIZGZ-UHFFFAOYSA-N;AKOS015918883;1(2H)-Pyridinecarboxylic acid, 3,4-dihydro-2-methyl-4-oxo-, phenylmethyl ester;A4211;FT-0654293;J-519785;2(R,S)-methyl-1(benzyloxycarbonyl)-2,3-dihydro-4-pyridone;2(R,S)-methyl-1-(benzyloxycarbonyl)-2,3-dihydro-4-pyridone;phenylmethyl 2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate;Racemic Benzyl 2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate

Suppliers and Price of benzyl 2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
Benzyl2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate 95
1g
$ 462.00

Crysdot
Benzyl2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate 95+%
1g
$ 396.00

Crysdot
Benzyl2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate 95+%
250mg
$ 158.00

Crysdot
Benzyl2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate 95+%
10g
$ 1984.00

Crysdot
Benzyl2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate 95+%
5g
$ 1191.00

Chemenu
benzyl2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate 95%
5g
$ 1122.00

Chemenu
benzyl2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate 95%
1g
$ 374.00

Biosynth Carbosynth
Benzyl2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate
100 mg
$ 112.00

Biosynth Carbosynth
Benzyl2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate
50 mg
$ 64.00

Biosynth Carbosynth
Benzyl2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate
250 mg
$ 222.50

Total 25 raw suppliers

Chemical Property of benzyl 2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Melting Point:52-54°C
Refractive Index:1.56
Boiling Point:385.746 °C at 760 mmHg
Flash Point:187.093 °C
PSA：46.61000
Density:1.193 g/cm³
LogP:2.43810
Storage Temp.:2-8°C
XLogP3:1.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:245.10519334
Heavy Atom Count:18
Complexity:345

Purity/Quality:

97% ^*data from raw suppliers

Benzyl2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CC(=O)C=CN1C(=O)OCC2=CC=CC=C2

Technology Process of benzyl 2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate

There total 4 articles about benzyl 2-methyl-4-oxo-3,4-dihydropyridine-1(2H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 620-08-6,1232006-56-2
4-methoxypyridine

: 75-16-1
methylmagnesium bromide

: 501-53-1,94274-21-2
benzyl chloroformate

: 190906-91-3
3,4-dihydro-2-methyl-4-oxo-1(2H)-pyridinecarboxylic acid phenylmethyl ester

Guidance literature:: 4-methoxypyridine; benzyl chloroformate; With triethylamine; In tetrahydrofuran; at -40 ℃; for 0.333333h;

methylmagnesium bromide; In tetrahydrofuran; diethyl ether; at 20 ℃; for 2h; Inert atmosphere;

Reference yield:

: 620-08-6,1232006-56-2
4-methoxypyridine

: 676-58-4
methylmagnesium chloride

: 501-53-1,94274-21-2
benzyl chloroformate

: 190906-91-3
3,4-dihydro-2-methyl-4-oxo-1(2H)-pyridinecarboxylic acid phenylmethyl ester

Guidance literature:: 4-methoxypyridine; benzyl chloroformate; In tetrahydrofuran; at -10 - -5 ℃; Inert atmosphere;

methylmagnesium chloride; In tetrahydrofuran; at -10 - -5 ℃; for 2h; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 0.166667h; Inert atmosphere;