Technology Process of Methyl phenanthrene-2-carboxylate
There total 9 articles about Methyl phenanthrene-2-carboxylate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
boron trifluoride;
for 6h;
Heating;
- Guidance literature:
-
With
silver(I) hexafluorophosphate; [dichloro(p-cymene)(triphenylphosphane)ruthenium(II)];
In
chlorobenzene;
at -78 - 120 ℃;
for 20h;
Inert atmosphere;
DOI:10.1002/chem.201500248
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 14 percent / aluminium chloride / nitrobenzene / 8.5 h / 0 - 25 °C
2: 55 percent / 2percent sodium hypochlorite / H2O / 24 h / Heating
3: 87 percent / 12percent boron trifluoride / 6 h / Heating
With
sodium hypochlorite; aluminium trichloride; boron trifluoride;
In
water; nitrobenzene;
