(2R,3s,4S)dimethyl 2,3,4-triacetoxyglutarate

Base Information

Chemical Name:(2R,3s,4S)dimethyl 2,3,4-triacetoxyglutarate
CAS No.:63181-60-2
Molecular Formula:C₁₃H₁₈O₁₀
Molecular Weight:334.28
Hs Code.:

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Chemical Property of (2R,3s,4S)dimethyl 2,3,4-triacetoxyglutarate

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Technology Process of (2R,3s,4S)dimethyl 2,3,4-triacetoxyglutarate

There total 1 articles about (2R,3s,4S)dimethyl 2,3,4-triacetoxyglutarate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 42859-41-6
methyl 2,4-di-O-acetyl-3,6-anhydro-α-D-galactopyranoside

: 6304-92-3
di-O-acetyltartaric acid dimethyl ester

: 63181-60-2,74033-70-8
tri-O-acetylarabinaric acid dimethyl ester

: 32786-27-9
O-acetyltartronic acid dimethyl ester

Guidance literature:: With chromium(VI) oxide; hydrogenchloride; acetic anhydride; acetyl chloride; Product distribution; multistep reaction: 1.) 20 deg C, 30 min, 2.) reflux, 0.5 h; CrO₃ oxidation of anomeric methyl galactopyranosides, effect of the anomeric centre confuguration on the rate of oxidation; effect of the temperature and time on the degree of oxidation;
DOI:10.1007/BF00961769